N1-Ethyl-4-nitrobenzene-1,2-diamine

Base Information

Chemical Name:N1-Ethyl-4-nitrobenzene-1,2-diamine
CAS No.:66668-41-5
Molecular Formula:C8H11N3O2
Molecular Weight:181.194
Hs Code.:2921590090
DSSTox Substance ID:DTXSID90404891
Wikidata:Q82209233

Synonyms:N1-Ethyl-4-nitrobenzene-1,2-diamine;66668-41-5;1-N-ethyl-4-nitrobenzene-1,2-diamine;N-ethyl-4-nitro-benzene-1,2-diamine;2-ethylamino-5-nitroaniline;SCHEMBL4978573;DTXSID90404891;PNDJSMFFLOHKTJ-UHFFFAOYSA-N;MFCD00156345;AKOS000271083;CS-0315700;FT-0758588;D84544;N1-ETHYL-4-NITRO-1,2-PHENYLENEDIAMINE

Suppliers and Price of N1-Ethyl-4-nitrobenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N1-ETHYL-4-NITRO-1,2-PHENYLENEDIAMINE Aldrich
1ea
$ 57.00

Crysdot
N1-Ethyl-4-nitrobenzene-1,2-diamine 95+%
1g
$ 377.00

American Custom Chemicals Corporation
N1-ETHYL-4-NITROBENZENE-1,2-DIAMINE 95.00%
5MG
$ 501.03

Alichem
N1-Ethyl-4-nitrobenzene-1,2-diamine
1g
$ 338.80

Total 8 raw suppliers

Chemical Property of N1-Ethyl-4-nitrobenzene-1,2-diamine

Chemical Property:

Vapor Pressure:9.44E-06mmHg at 25°C
Boiling Point:372.7°C at 760 mmHg
Flash Point:179.2°C
PSA：83.87000
Density:1.298g/cm³
LogP:2.78620
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:181.085126602
Heavy Atom Count:13
Complexity:181

Purity/Quality:

98%,99%, ^*data from raw suppliers

N1-ETHYL-4-NITRO-1,2-PHENYLENEDIAMINE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCNC1=C(C=C(C=C1)[N+](=O)[O-])N

Technology Process of N1-Ethyl-4-nitrobenzene-1,2-diamine

There total 5 articles about N1-Ethyl-4-nitrobenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3846-50-2
2,4-dinitro-N-ethylaniline

: 66668-41-5
N¹-ethyl-4-nitro-benzene-1,2-diamine

Guidance literature:: With nickel; hydrazine hydrate; In ethanol; 1,2-dichloro-ethane; at 50 - 60 ℃; for 6h;
DOI:10.1246/bcsj.56.3159

Reference yield: 72.0%

: 66668-41-5
N¹-ethyl-4-nitro-benzene-1,2-diamine

Guidance literature:

Reference yield:

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 66668-41-5
N¹-ethyl-4-nitro-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / CH₃COONa*3H₂O / ethanol / 2 h / Heating

2: 69 percent / Na₂S*9H₂O; sulfur / ethanol; H₂O / 2 h / Heating

With sodium sulfide; sodium acetate; sulfur; In ethanol; water;
DOI:10.1134/S1070363206080214