1-(4-CHLORO-PHENYL)-2,2,2-TRIFLUORO-ETHYLAMINE

Base Information

• Chemical Name: 1-(4-CHLORO-PHENYL)-2,2,2-TRIFLUORO-ETHYLAMINE
• CAS No.: 65686-86-4
• Molecular Formula: C₈H₇ClF₃N
• Molecular Weight: 209.598
• Hs Code.: 2921499090
• Mol file: 65686-86-4.mol

Synonyms:Benzenemethanamine, 4-chloro-.alpha.-(trifluoromethyl)-;

Chemical Property of 1-(4-CHLORO-PHENYL)-2,2,2-TRIFLUORO-ETHYLAMINE

Chemical Property:

• Vapor Pressure: 0.0427mmHg at 25°C
• Boiling Point: 238.3°C at 760 mmHg
• Flash Point: 97.9°C
• PSA: 26.02000
• Density: 1.352g/cm³
• LogP: 3.60240
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-(4-chlorophenyl)-2,2,2-trifluoroethanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-CHLORO-PHENYL)-2,2,2-TRIFLUORO-ETHYLAMINE

There total 3 articles about 1-(4-CHLORO-PHENYL)-2,2,2-TRIFLUORO-ETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methyl-propane-2-sulfinic acid [(S)-1-(4-chloro-phenyl)-2,2,2-trifluoro-ethyl]-amide → [α-(4-chlorophenyl) trifluoroethyl] amine (65686-86-4,766498-73-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 1h;

DOI:10.1039/c6cc10124k

Reference yield:

4'-chloro-2,2,2-trifluoroacetophenone (321-37-9) → [α-(4-chlorophenyl) trifluoroethyl] amine (65686-86-4,766498-73-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: titanium(IV) isopropylate / diethyl ether / 24 h / 50 °C

1.2: 3 h / -20 °C

2.1: hydrogenchloride / 1,4-dioxane; methanol / 1 h / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; In 1,4-dioxane; methanol; diethyl ether;

DOI:10.1039/c6cc10124k

Reference yield:

→ [α-(4-chlorophenyl) trifluoroethyl] amine (65686-86-4,766498-73-1)

Guidance literature:

upstream raw materials:

4'-chloro-2,2,2-trifluoroacetophenone

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