3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide

Base Information

• Chemical Name: 3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide
• CAS No.: 152811-37-5
• Molecular Formula: C57H59BrO14
• Molecular Weight: 1047.97396
• European Community (EC) Number: 678-085-4
• DSSTox Substance ID: DTXSID10579176
• Nikkaji Number: J1.976.778G
• Wikidata: Q82469615
• Mol file: 152811-37-5.mol

Synonyms:3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide;152811-37-5;1,3-bis[[3,5-bis[(3,5-dimethoxyphenyl)methoxy]phenyl]methoxy]-5-(bromomethyl)benzene;BMISSUNAKMQTFS-UHFFFAOYSA-N;DTXSID10579176;MFCD14708165;AKOS015851729;B2248;CS-0435409;T70325;3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzylBromide;1,1',1'',1'''-{[5-(Bromomethyl)-1,3-phenylene]bis[oxymethylenebenzene-5,1,3-triylbis(oxymethylene)]}tetrakis(3,5-dimethoxybenzene);5,5',5'',5'''-((((((5-(Bromomethyl)-1,3-phenylene)bis(oxy))bis(methylene))bis(benzene-5,3,1-triyl))tetrakis(oxy))tetrakis(methylene))tetrakis(1,3-dimethoxybenzene)

Chemical Property of 3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 1043.432°C at 760 mmHg
• Flash Point: 450.642°C
• PSA: 129.22000
• Density: 1.279g/cm³
• LogP: 12.12430
• Storage Temp.: 0-10°C
• XLogP3: 11
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 14
• Rotatable Bond Count: 27
• Exact Mass: 1046.30882
• Heavy Atom Count: 72
• Complexity: 1230

Purity/Quality:

97% ^*data from raw suppliers

3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide >97.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=CC(=C1)COC2=CC(=CC(=C2)COC3=CC(=CC(=C3)CBr)OCC4=CC(=CC(=C4)OCC5=CC(=CC(=C5)OC)OC)OCC6=CC(=CC(=C6)OC)OC)OCC7=CC(=CC(=C7)OC)OC)OC

Technology Process of 3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide

There total 1 articles about 3,5-Bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyl Bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

{3,5-bis-[3,5-bis-(3,5-dimethoxy-benzyloxy)-benzyloxy]-phenyl}-methanol → 3,5-bis{3,5-bis(3,5-dimethoxybenzyloxy)-benzyloxy}benzyl bromide (152811-37-5)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1039/b812503a

Reference yield:

Bis<2-(N,N-dimethylamino)aethyl>aether (3033-62-3) + 3,5-bis{3,5-bis(3,5-dimethoxybenzyloxy)-benzyloxy}benzyl bromide (152811-37-5) → 2,2'-oxybis(N-[3,5-bis{3,5-bis(3,5-dimethoxybenzyloxy)-benzyloxy}benzyloxy]-N,N-dimethylethanaminium) dibromide

Guidance literature:

In N,N-dimethyl-formamide; at 70 ℃; for 15h; Inert atmosphere;

DOI:10.1248/cpb.c12-00682

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