Pyridine, 2,5-bis(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Pyridine, 2,5-bis(2,4,6-trimethylphenyl)-
CAS No.:1312698-01-3
Molecular Formula:C23H25N
Molecular Weight:315.458
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyridine, 2,5-bis(2,4,6-trimethylphenyl)-

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Technology Process of Pyridine, 2,5-bis(2,4,6-trimethylphenyl)-

There total 1 articles about Pyridine, 2,5-bis(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 624-28-2
2,5-dibromopyridine

: 2633-66-1
2-mesitylmagnesium bromide

: 1312698-01-3
2,5-dimesitylpyridine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 0 - 75 ℃; Inert atmosphere;
DOI:10.1021/ic201205p

Reference yield: 74.0%

: 1312698-01-3
2,5-dimesitylpyridine

: cobalt(II) iodide

: 1312697-97-4
[Co(iodide)2(2,5-dimesitylpyridine)]2

Guidance literature:: In tetrahydrofuran; (N2), Schlenk techniques; addn. of soln. of Co compd. in THF to soln. ofN compd. in THF, stirring for 36 h; filtration (Celite), evapn. under reduced pressure, washing with n-pentane, drying under reduced pressure, dissolving in toluene/n-pentane/THF (2:2:1), filtration, storage at -35°C for 24 h, isolation of crystals, drying in vacuo, elem. anal.;
DOI:10.1021/ic201205p

Reference yield: 69.0%

: 37234-97-2
copper(I) trifluoromethanesulfonate benzene

: 1312698-01-3
2,5-dimesitylpyridine

: 1312697-94-1
[Cu(2,5-dimesitylpyridine)2]OTf

Guidance literature:: In tetrahydrofuran; (N2), Schlenk techniques; at room temp. addn. of soln. of N compd. in THF to soln. of Cu compd. in THF, stirring for 36 h; filtration (Celite), evapn. under reduced pressure, dissolving in toluene/n-pentane (2:1), filtration, storage at -35°C for 24 h, isolation of crystals, drying in vacuo, elem. anal.;
DOI:10.1021/ic201205p