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9,12-Methano-1H-diindolo[1,2,3-fg:3',2',1'-kl]pyrrolo[3,4-i][1,6]benzodia zocine-1,3(2H)-dione, 9,12-dihydro-2-[(4-methoxyphenyl)methyl]-

Base Information
  • Chemical Name:9,12-Methano-1H-diindolo[1,2,3-fg:3',2',1'-kl]pyrrolo[3,4-i][1,6]benzodia zocine-1,3(2H)-dione, 9,12-dihydro-2-[(4-methoxyphenyl)methyl]-
  • CAS No.:253680-52-3
  • Molecular Formula:C33H23N3O3
  • Molecular Weight:509.564
  • Hs Code.:
9,12-Methano-1H-diindolo[1,2,3-fg:3',2',1'-kl]pyrrolo[3,4-i][1,6]benzodia zocine-1,3(2H)-dione, 9,12-dihydro-2-[(4-methoxyphenyl)methyl]-

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Chemical Property of 9,12-Methano-1H-diindolo[1,2,3-fg:3',2',1'-kl]pyrrolo[3,4-i][1,6]benzodia zocine-1,3(2H)-dione, 9,12-dihydro-2-[(4-methoxyphenyl)methyl]-
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Technology Process of 9,12-Methano-1H-diindolo[1,2,3-fg:3',2',1'-kl]pyrrolo[3,4-i][1,6]benzodia zocine-1,3(2H)-dione, 9,12-dihydro-2-[(4-methoxyphenyl)methyl]-

There total 1 articles about 9,12-Methano-1H-diindolo[1,2,3-fg:3',2',1'-kl]pyrrolo[3,4-i][1,6]benzodia zocine-1,3(2H)-dione, 9,12-dihydro-2-[(4-methoxyphenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C28H19N3O3; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.75h;
cis-3,5-dibromocyclopentene; In tetrahydrofuran; at 0 ℃; for 0.833333h;
With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield: 86.4%

Guidance literature:
C33H23N3O3; With borane-THF; In tetrahydrofuran; at 20 ℃;
With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 0 ℃; for 1.5h; Alkaline aqueous solution;

Reference yield: 69.0%

Guidance literature:
With 4-methylmorpholine N-oxide; osmium(VIII) oxide; In water; acetone; at 20 ℃; for 2h;
upstream raw materials:

cis-3,5-dibromocyclopentene

C28H19N3O3

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