Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(2,3,4,5,6-pentachlorophenyl)-

Base Information

Chemical Name:Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(2,3,4,5,6-pentachlorophenyl)-
CAS No.:128083-22-7
Molecular Formula:C24Br2Cl18Ge
Molecular Weight:1158.82
Hs Code.:

Synonyms:Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(pentachlorophenyl)- (9CI);

Suppliers and Price of Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(2,3,4,5,6-pentachlorophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(2,3,4,5,6-pentachlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(2,3,4,5,6-pentachlorophenyl)-

There total 2 articles about Germane, bromo(2'-bromo-3,3',4,4',5,5',6,6'-octachloro[1,1'-biphenyl]-2-yl)bis(2,3,4,5,6-pentachlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 128083-21-6
perchloro(2,2'-biphenylene)diphenylgermane

: 128083-22-7
bromo(2-(2'-bromooctachlorobiphenyl)bis(pentachlorophenyl))germane

Guidance literature:: With Br₂; In tetrachloromethane; Irradiation (UV/VIS); a mixt. of the Ge-complex and Br2 in CCl4 refluxed for 13h with illumination from a 500 W incandescent lamp; evapd. to dryness in vac., Br2 removed, digestion with boiling C6H6 and CHCl3; elem. anal.;
DOI:10.1016/0022-328X(90)80062-5

Reference yield:

: 31279-13-7
pentachlorophenylmagnesium chloride

: 128083-22-7
bromo(2-(2'-bromooctachlorobiphenyl)bis(pentachlorophenyl))germane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: Br₂ / tetrachloromethane

With Br₂; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/0022-328X(90)80062-5