Carbonodithioic acid, S-[2-(4-chlorophenyl)-2-(hydroxyimino)ethyl] O-ethyl ester

Base Information

Chemical Name:Carbonodithioic acid, S-[2-(4-chlorophenyl)-2-(hydroxyimino)ethyl] O-ethyl ester
CAS No.:195213-53-7
Molecular Formula:C11H12ClNO2S2
Molecular Weight:289.807
Hs Code.:

Synonyms:

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Chemical Property of Carbonodithioic acid, S-[2-(4-chlorophenyl)-2-(hydroxyimino)ethyl] O-ethyl ester

Chemical Property:

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Technology Process of Carbonodithioic acid, S-[2-(4-chlorophenyl)-2-(hydroxyimino)ethyl] O-ethyl ester

There total 4 articles about Carbonodithioic acid, S-[2-(4-chlorophenyl)-2-(hydroxyimino)ethyl] O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 136978-96-6
ω-bromo-p-chloroacetophenone oxime

: 140-89-6
potassium ethyl xanthogenate

: 195213-53-7
O-ethyl S-<2-(p-chlorophenyl)ethyl-2-oximino> dithiocarbonate

Guidance literature:: In acetone;
DOI:10.1055/s-1997-5754

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 195213-53-7
O-ethyl S-<2-(p-chlorophenyl)ethyl-2-oximino> dithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / hydroxylamine hydrochloride / methanol

2: 97 percent / acetone

With hydroxylamine hydrochloride; In methanol; acetone;
DOI:10.1055/s-1997-5754

Reference yield:

: 99-91-2
para-chloroacetophenone

: 195213-53-7
O-ethyl S-<2-(p-chlorophenyl)ethyl-2-oximino> dithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; hydrogen bromide; bromine / 2.25 h / 15 - 25 °C

2: hydroxylamine hydrochloride / ethanol; water / 24 h / 20 °C

3: acetone / 3.5 h / 20 °C

With hydroxylamine hydrochloride; hydrogen bromide; bromine; acetic acid; In ethanol; water; acetone;
DOI:10.15227/orgsyn.079.0228