3-oxa-9-azaspiro[5.5]undecane(SALTDATA: FREE)

Base Information

• Chemical Name: 3-oxa-9-azaspiro[5.5]undecane(SALTDATA: FREE)
• CAS No.: 311-21-7
• Molecular Formula: C9H17NO
• Molecular Weight: 155.24
• Hs Code.: 2934999090
• Mol file: 311-21-7.mol

Synonyms:3-Oxa-9-azaspiro[5.5]undecane;3-oxa-9-azaspiro 5.5 undecane(SALTDATA;3-Oxa-9-azaspiro[5.5]undecane - X10643;3-Oxa-9-azaspiro[5.5]undecane (8CI,9CI);3-Oxa-9-azaspiro[5.5]undecane heMioxalate;3-oxa-9-azaspiro[5.5]undecane(SALTDATA: FREE);3-Oxa-9-azaspiro[5.5]undecane hydrochloride salt

Chemical Property of 3-oxa-9-azaspiro[5.5]undecane(SALTDATA: FREE)

Chemical Property:

• Boiling Point: 250℃
• PKA: 10.94±0.20(Predicted)
• Flash Point: 96℃
• PSA: 21.26000
• Density: 1.00
• LogP: 1.49540
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

3-oxa-9-azaspiro[5.5]undecane ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-oxa-9-azaspiro[5.5]undecane(SALTDATA: FREE)

There total 1 articles about 3-oxa-9-azaspiro[5.5]undecane(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-azaspiro[5.5]undecane-9-carboxylic acid → 3-oxa-9-azaspiro[5.5]undecane (311-21-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

Reference yield: 96.0%

3-oxa-9-azaspiro[5.5]undecane (311-21-7) + C18H17N3O3 → 1-benzyl-N-[3-(3-oxa-9-azaspiro[5.5]undec-9-yl)-3-oxopropyl]-1H-benzimidazole-2-carboxamide

Guidance literature:

With 2-chloro-1,3-dimethylimidazolinium chloride; N-ethyl-N,N-diisopropylamine; In acetonitrile;

DOI:10.1016/j.bmcl.2008.08.014

Reference yield: 81.18%

2-(chloromethyl)-5-(4-nitrophenyl)-1,3,4-oxadiazole (50677-30-0) + 3-oxa-9-azaspiro[5.5]undecane (311-21-7) → 9-((5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl)methyl)-3-oxa-9-azaspiro[5.5]undecane

Guidance literature:

3-oxa-9-azaspiro[5.5]undecane; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.25h;

2-(chloromethyl)-5-(4-nitrophenyl)-1,3,4-oxadiazole; With sodium iodide; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1002/jhet.4200

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