5 - Methylpicolinic acid hydrochloride

Base Information

• Chemical Name: 5 - Methylpicolinic acid hydrochloride
• CAS No.: 177359-60-3
• Molecular Formula: C7H7NO2.ClH
• Molecular Weight: 173.59692
• Hs Code.: 2933399090
• Mol file: 177359-60-3.mol

Synonyms:5 - Methylpicolinic acid hydrochloride;5-Methylpyridine-2-carboxylic acid hydrochloride

Chemical Property of 5 - Methylpicolinic acid hydrochloride

Chemical Property:

• PSA: 50.19000
• LogP: 1.89020
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

5-methylpyridine-2-carboxylicacidhydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5 - Methylpicolinic acid hydrochloride

There total 3 articles about 5 - Methylpicolinic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

5-methyl-2-pyridinecarboxylic acid-ethyl ester (55876-82-9) → 5-methyl-pyridine-2-carboxylic acid hydrochloride (177359-60-3)

Guidance literature:

In 6N-hydrochloric acid; acetonitrile;

Reference yield:

5-methylpicolinonitrile (1620-77-5) → 5-methyl-pyridine-2-carboxylic acid hydrochloride (177359-60-3)

Guidance literature:

With hydrogenchloride; In ethanol; water; for 40h; Heating / reflux;

Reference yield:

2-Bromo-5-methylpyridine (3510-66-5) → 5-methyl-pyridine-2-carboxylic acid hydrochloride (177359-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc(II) cyanide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; zinc / DMF (N,N-dimethyl-formamide) / 0.25 h / 155 °C

2: hydrogenchloride / ethanol; water / 40 h / Heating / reflux

With zinc(II) cyanide; hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; zinc; In DMF (N,N-dimethyl-formamide); ethanol; water;

upstream raw materials:

5-methylpicolinonitrile

5-methyl-2-pyridinecarboxylic acid-ethyl ester

2-Bromo-5-methylpyridine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 177359-60-3 5 - Methylpicolinic acid hydrochloride

Send

Send

Metric Ton KG G Pound L ML

Send

Send