TERT-BUTYL 1-OXO-2,7-DIAZASPIRO[3.5]NONANE-7-CARBOXYLATE

Base Information

• Chemical Name: TERT-BUTYL 1-OXO-2,7-DIAZASPIRO[3.5]NONANE-7-CARBOXYLATE
• CAS No.: 1032158-48-7
• Molecular Formula: C12H20N2O3
• Molecular Weight: 240.2988
• Hs Code.: 2933990090
• Mol file: 1032158-48-7.mol

Synonyms:TERT-BUTYL 1-OXO-2,7-DIAZASPIRO[3.5]NONANE-7-CARBOXYLATE;7-Boc-1-oxo-2,7-diazaspiro[3.5]nonane;1-Oxo-2,7-diaza-spiro[3.5]nonane-7-carboxylic acid tert-butyl ester;2,7-Diazaspiro[3.5]nonane-7-carboxylic acid, 1-oxo-, 1,1-diMethylethyl ester

Chemical Property of TERT-BUTYL 1-OXO-2,7-DIAZASPIRO[3.5]NONANE-7-CARBOXYLATE

Chemical Property:

• Melting Point: 1.17℃
• Boiling Point: 412℃
• PKA: 14.82±0.20(Predicted)
• Flash Point: 203℃
• PSA: 32.78000
• Density: 1.17±0.1 g/cm3(Predicted)
• LogP: 1.82490
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl1-Oxo-2,7-diazaspiro[3.5]nonane-7-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL 1-OXO-2,7-DIAZASPIRO[3.5]NONANE-7-CARBOXYLATE

There total 1 articles about TERT-BUTYL 1-OXO-2,7-DIAZASPIRO[3.5]NONANE-7-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 2-(4-methoxybenzyl)-1-oxo-2,7-diazaspiro[3.5]nonane-7-carboxylate → tert-butyl 1-oxo-2,7-diazaspiro[3.5]nonane-7-carboxylate (1032158-48-7)

Guidance literature:

With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; for 0.5h;

Reference yield:

C18H14BrNO2 (959960-87-3) + tert-butyl 1-oxo-2,7-diazaspiro[3.5]nonane-7-carboxylate (1032158-48-7) → C30H33N3O5 (1032158-32-9)

Guidance literature:

With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; N,N-dimethyl-formamide; at 175 ℃; for 0.333333h; Microwave irradiation;

Reference yield:

tert-butyl 1-oxo-2,7-diazaspiro[3.5]nonane-7-carboxylate (1032158-48-7) → 2.7-diaza-spiro[3.5]nonan-1-one (1147422-92-1)

Guidance literature:

tert-butyl 1-oxo-2,7-diazaspiro[3.5]nonane-7-carboxylate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With ammonia; In methanol;

Downstream raw materials:

C₃₀H₃₃N₃O₅

2.7-diaza-spiro[3.5]nonan-1-one

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