1H-INDOLE-3-CARBOXYLIC ACID,7-FLUORO

Base Information

• Chemical Name: 1H-INDOLE-3-CARBOXYLIC ACID,7-FLUORO
• CAS No.: 858515-66-9
• Molecular Formula: C₉H₆FNO₂
• Molecular Weight: 179.151
• Hs Code.: 2933998090
• Mol file: 858515-66-9.mol

Synonyms:1H-INDOLE-3-CARBOXYLIC ACID,7-FLUORO;7-Fluoro-indole-3-carboxylic acid;7-Fluoro-1H-indole-3-carboxylic acid

Chemical Property of 1H-INDOLE-3-CARBOXYLIC ACID,7-FLUORO

Chemical Property:

• PSA: 53.09000
• LogP: 2.00520
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

1H-INDOLE-3-CARBOXYLICACID,7-FLUORO 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-INDOLE-3-CARBOXYLIC ACID,7-FLUORO

There total 3 articles about 1H-INDOLE-3-CARBOXYLIC ACID,7-FLUORO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

→ 7-fluoro-1H-indole-3-carboxylic acid (858515-66-9)

Guidance literature:

In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

7-fluoro-1H-indole (387-44-0) → 7-fluoro-1H-indole-3-carboxylic acid (858515-66-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide

2: aq. NaOH

With sodium hydroxide; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2005.04.002

Reference yield:

2,2,2-trifluoro-1-(7-fluoro-1H-indol-3-yl)-ethanone (858515-94-3) → 7-fluoro-1H-indole-3-carboxylic acid (858515-66-9)

Guidance literature:

With sodium hydroxide;

DOI:10.1016/j.bmcl.2005.04.002

upstream raw materials:

2,2,2-trifluoro-1-(7-fluoro-1H-indol-3-yl)-ethanone

7-fluoro-1H-indole

Downstream raw materials:

C₃₁H₃₈FN₃O₅

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