L-Phenylalanine, β-methyl-, hydrochloride, (βS)- (9CI)

Base Information

Chemical Name:L-Phenylalanine, β-methyl-, hydrochloride, (βS)- (9CI)
CAS No.:53331-55-8
Molecular Formula:C10H13NO2.ClH
Molecular Weight:215.68
Hs Code.:
Mol file:53331-55-8.mol

Synonyms:L-Phenylalanine, β-methyl-, hydrochloride, erythro-;erythro-L-β-Methylphenylalanine hydrochloride;

Suppliers and Price of L-Phenylalanine, β-methyl-, hydrochloride, (βS)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of L-Phenylalanine, β-methyl-, hydrochloride, (βS)- (9CI)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of L-Phenylalanine, β-methyl-, hydrochloride, (βS)- (9CI)

There total 11 articles about L-Phenylalanine, β-methyl-, hydrochloride, (βS)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 954111-43-4
C₂₁H₂₅NO₃

: 53331-55-8,59850-51-0
(2S,3S)-β-methylphenylalanine hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 100 ℃; for 9h;
DOI:10.1021/ol701558e

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 53331-55-8,59850-51-0
(2S,3S)-β-methylphenylalanine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: (R)-BINAP; [Rh(COD)2]⁺BF₄^- / 1,2-dimethoxy-ethane / 4 h / -78 °C

2.1: 1,2-dimethoxy-ethane / -78 - 20 °C

3.1: LAH / diethyl ether / 1 h / 0 °C

3.2: TMSCl / diethyl ether / 13 h / 0 - 20 °C

4.1: cinchonine; nBuLi; LiCl / tetrahydrofuran / 13 h / 0 - 20 °C

5.1: HCl / CHCl₃; H₂O

With hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; lithium chloride; Cinchonin; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; chloroform; water;
DOI:10.1021/ja0298794