Benzenepropanoic acid, 5-[4-(cyclopentyloxy)-2-hydroxybenzoyl]-2-[[2,3-dihydro-3-oxo-2-(triphenylmethyl)-1,2-benzisoxazol-6-yl]methoxy]-, methyl ester

Base Information

Chemical Name:Benzenepropanoic acid, 5-[4-(cyclopentyloxy)-2-hydroxybenzoyl]-2-[[2,3-dihydro-3-oxo-2-(triphenylmethyl)-1,2-benzisoxazol-6-yl]methoxy]-, methyl ester
CAS No.:947409-01-0
Molecular Formula:C49H43NO8
Molecular Weight:773.882
Hs Code.:

Benzenepropanoic acid, 5-[4-(cyclopentyloxy)-2-hydroxybenzoyl]-2-[[2,3-dihydro-3-oxo-2-(triphenylmethyl)-1,2-benzisoxazol-6-yl]methoxy]-, methyl ester

Synonyms:3-[5-[4-(Cyclopentyloxy)-2-hydroxybenzoyl]-2-[(3-oxo-2-triphenylmethyl-2,3-dihydro-1,2-benzisoxazol-6-yl)methoxy]phenyl]propionic acid methyl ester;

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Chemical Property of Benzenepropanoic acid, 5-[4-(cyclopentyloxy)-2-hydroxybenzoyl]-2-[[2,3-dihydro-3-oxo-2-(triphenylmethyl)-1,2-benzisoxazol-6-yl]methoxy]-, methyl ester

Chemical Property:

PSA：117.20000
LogP:9.37730

Purity/Quality:

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Technology Process of Benzenepropanoic acid, 5-[4-(cyclopentyloxy)-2-hydroxybenzoyl]-2-[[2,3-dihydro-3-oxo-2-(triphenylmethyl)-1,2-benzisoxazol-6-yl]methoxy]-, methyl ester

There total 18 articles about Benzenepropanoic acid, 5-[4-(cyclopentyloxy)-2-hydroxybenzoyl]-2-[[2,3-dihydro-3-oxo-2-(triphenylmethyl)-1,2-benzisoxazol-6-yl]methoxy]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

: 530141-60-7
methyl 3-[2-hydroxy-5-(2-hydroxy-4-cyclopentyloxybenzoyl)phenyl]propionate

: 947408-95-9
2-trityl-6-bromomethylbenzisoxazol-3-one

: 947409-01-0
methyl 3-[2-[(2-trityl-3-keto-benzisoxazol-6-yl)methoxy]-5-(2-hydroxy-4-cyclopentyloxybenzoyl)phenyl]propionate

Guidance literature:: With potassium carbonate; In acetone; for 5h; Reflux;

Reference yield:

: 947408-91-5
6-(2,4-dihydroxybenzoyl)chromen-2-one

: 947409-01-0
methyl 3-[2-[(2-trityl-3-keto-benzisoxazol-6-yl)methoxy]-5-(2-hydroxy-4-cyclopentyloxybenzoyl)phenyl]propionate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

2: methanol / 4 h / 60 °C / Inert atmosphere

3: sodium formate; acetic acid; 5%-palladium/activated carbon / isopropyl alcohol; water / 5 h / 45 °C

4: potassium carbonate / acetone / 5 h / Reflux

With 5%-palladium/activated carbon; sodium formate; potassium carbonate; acetic acid; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol; acetone;

Reference yield:

: 947408-90-4
6-(2,4-dimethoxybenzoyl)chromen-2-one

: 947409-01-0
methyl 3-[2-[(2-trityl-3-keto-benzisoxazol-6-yl)methoxy]-5-(2-hydroxy-4-cyclopentyloxybenzoyl)phenyl]propionate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine hydrochloride / 2 h / 200 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

3: methanol / 4 h / 60 °C / Inert atmosphere

4: sodium formate; acetic acid; 5%-palladium/activated carbon / isopropyl alcohol; water / 5 h / 45 °C

5: potassium carbonate / acetone / 5 h / Reflux

With 5%-palladium/activated carbon; sodium formate; pyridine hydrochloride; potassium carbonate; acetic acid; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol; acetone;