6,6'-difluoro-2,2'-bipyridine

Base Information

• Chemical Name: 6,6'-difluoro-2,2'-bipyridine
• CAS No.: 616225-38-8
• Molecular Formula: C₁₀H₆F₂N₂
• Molecular Weight: 192.168
• Hs Code.: 2933399090
• Mol file: 616225-38-8.mol

Synonyms:6,6'-DIFLUORO-2,2'-BIPYRIDINE;

Chemical Property of 6,6'-difluoro-2,2'-bipyridine

Chemical Property:

• PSA: 25.78000
• LogP: 2.42180

Purity/Quality:

97% ^*data from raw suppliers

6,6'-Difluoro-2,2'-bipyridine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6,6'-difluoro-2,2'-bipyridine

There total 2 articles about 6,6'-difluoro-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N,N’-difluoro-2,2’-bipyridinium bis(tetrafluoroborate) → 6,6’-difluoro-2,2’-bipyridine (616225-38-8)

Guidance literature:

With triethylamine; at 25 ℃; for 1h;

DOI:10.1055/s-2003-39173

Reference yield: 5.0%

2-bromo-6-fluoropyridine (144100-07-2) → 6,6’-difluoro-2,2’-bipyridine (616225-38-8)

Guidance literature:

With palladium diacetate; potassium carbonate; at 120 ℃; for 48h;

DOI:10.1039/c8dt05159c

upstream raw materials:

2-bromo-6-fluoropyridine