6-(3,4-DiMethoxyphenyl)-3-pyridinecarbaldehyde

Base Information

• Chemical Name: 6-(3,4-DiMethoxyphenyl)-3-pyridinecarbaldehyde
• CAS No.: 898796-17-3
• Molecular Formula: C14H13NO3
• Molecular Weight: 243.25792
• Hs Code.: 2933399990
• Mol file: 898796-17-3.mol

Synonyms:6-(3,4-DiMethoxyphenyl)-3-pyridinecarbaldehyde

Chemical Property of 6-(3,4-DiMethoxyphenyl)-3-pyridinecarbaldehyde

Chemical Property:

• PSA: 48.42000
• LogP: 2.57830

Purity/Quality:

97% ^*data from raw suppliers

6-(3,4-Dimethoxyphenyl)-3-pyridinecarbaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-(3,4-DiMethoxyphenyl)-3-pyridinecarbaldehyde

There total 2 articles about 6-(3,4-DiMethoxyphenyl)-3-pyridinecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

3,4-Dimethoxyphenylboronic acid (122775-35-3) + 6-bromonicotinaldehyde (149806-06-4) → 2-(3,4-dimethoxyphenyl)-5-formylpyridine (898796-17-3)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate tribasic; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; water; at 100 ℃; for 16h; Inert atmosphere; Sealed tube;

DOI:10.1021/jm901469p

Reference yield: 77.0%

→ 2-(3,4-dimethoxyphenyl)-5-formylpyridine (898796-17-3)

Guidance literature:

Reference yield: 86.0%

(S)-2-(4-oxo-2-thioxothiazolidin-3-yl)-3-phenylpropanoic acid (161192-25-2) + 2-(3,4-dimethoxyphenyl)-5-formylpyridine (898796-17-3) → C26H22N2O5S2*ClH (1208222-54-1)

Guidance literature:

(S)-2-(4-oxo-2-thioxothiazolidin-3-yl)-3-phenylpropanoic acid; 2-(3,4-dimethoxyphenyl)-5-formylpyridine; With sodium acetate; acetic acid; for 3h; Reflux;

With hydrogenchloride; In water; for 1h; Reflux;

DOI:10.1021/jm901469p

upstream raw materials:

3,4-Dimethoxyphenylboronic acid

6-bromonicotinaldehyde

Downstream raw materials:

C₂₆H₂₂N₂O₅S₂*ClH

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