trans-4-(trans-4-propylcyclohexyl) cyclohexyl Methylene chloride

Base Information

• Chemical Name: trans-4-(trans-4-propylcyclohexyl) cyclohexyl Methylene chloride
• CAS No.: 321308-90-1
• Molecular Formula: C16H29Cl
• Molecular Weight: 256.85
• Mol file: 321308-90-1.mol

Synonyms:(trans,trans)-4-(Chloromethyl)-4'-propyl-1,1'-bicyclohexyl;1,1'-Bicyclohexyl, 4-(chloromethyl)-4'-propyl-, (trans,trans)-;trans-4-(trans-4-propylcyclohexyl) cyclohexyl Methylene chloride

Chemical Property of trans-4-(trans-4-propylcyclohexyl) cyclohexyl Methylene chloride

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

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Technology Process of trans-4-(trans-4-propylcyclohexyl) cyclohexyl Methylene chloride

There total 1 articles about trans-4-(trans-4-propylcyclohexyl) cyclohexyl Methylene chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

trans-4-(trans-4-propylcyclohexyl)cyclohexylmethanol → trans-4-(trans-4-propylcyclohexyl)cyclohexyl-methyl chloride (321308-90-1)

Guidance literature:

With pyridine; sodium hydroxide; thionyl chloride; sodium hydrogencarbonate; In water; toluene;

Reference yield:

4-trans-chloromethyl-4'-trans-propyl-bicyclohexane (1384466-01-6,321308-90-1) → C29H33F7O2

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

2.1: sec.-butyllithium / tetrahydrofuran; hexane; cyclohexane / 1 h / -70 °C / Inert atmosphere

2.2: 8 h / -70 - 20 °C / Inert atmosphere

3.1: toluene; 2,2,4-trimethylpentane / 1 h / 60 °C / Inert atmosphere

3.2: 3 h / 60 °C / Inert atmosphere; Reflux

4.1: triethylamine / dichloromethane / 1 h / -70 °C / Inert atmosphere

4.2: 0.5 h / -70 °C / Inert atmosphere

4.3: 1 h / -70 °C / Inert atmosphere

With tetrabutylammomium bromide; sec.-butyllithium; potassium carbonate; triethylamine; In tetrahydrofuran; 2,2,4-trimethylpentane; hexane; dichloromethane; cyclohexane; N,N-dimethyl-formamide; toluene;

Reference yield:

4-trans-chloromethyl-4'-trans-propyl-bicyclohexane (1384466-01-6,321308-90-1) → C23H32F2O3

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

2.1: sec.-butyllithium / tetrahydrofuran; hexane; cyclohexane / 1 h / -70 °C / Inert atmosphere

2.2: 8 h / -70 - 20 °C / Inert atmosphere

With tetrabutylammomium bromide; sec.-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; cyclohexane; N,N-dimethyl-formamide;

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