Methyl 3-(bis{[(2-methyl-2-propanyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

Base Information

Chemical Name:Methyl 3-(bis{[(2-methyl-2-propanyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate
CAS No.:1019338-24-9
Molecular Formula:C16H22INO6S
Molecular Weight:483.324
Hs Code.:

Synonyms:methyl 3-[bis(tert-butoxycarbonyl)amino]-5-iodothiophene-2-carboxylate;

Suppliers and Price of Methyl 3-(bis{[(2-methyl-2-propanyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 3-(bis{[(2-methyl-2-propanyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

Chemical Property:

PSA：110.38000
LogP:4.81590

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methyl 3-(bis{[(2-methyl-2-propanyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

There total 1 articles about Methyl 3-(bis{[(2-methyl-2-propanyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849618-96-8
methyl 3-(bis{[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-thiophenecarboxylate

: 1019338-24-9
methyl 3-(bis{[(1,1-dimethylethyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

Guidance literature:: methyl 3-(bis{[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-thiophenecarboxylate; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 - -70 ℃;

With iodine; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 - -70 ℃;

With water; ammonium chloride; In tetrahydrofuran; n-heptane; ethylbenzene; at 20 ℃;

Reference yield: 18.0%

: 942589-50-6
2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-pyrazolo[1,5-a]pyrimidine

: 1019338-24-9
methyl 3-(bis{[(1,1-dimethylethyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

: 1243142-15-5
methyl 3-(bis[terbutoxycarbonyl]amino)-5-(4-pyrazolo[1,5-a]pyrimidin-2-yl-phenyl)-2-thiophenecarboxylate

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 100 ℃; for 3h;

Reference yield: 7.5%

: 1019338-24-9
methyl 3-(bis{[(1,1-dimethylethyl)oxy]carbonyl}amino)-5-iodo-2-thiophenecarboxylate

: 1071794-98-3
4-{[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethynyl}-1,3-thiazole

: 1243142-19-9
methyl 3-(bis[tertbutoxycarbonyl]amino)-5-(4-phenyl-ethynyl-1,3-thiazole)-2-thiophenecarboxylate

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 100 ℃; for 3.5h; Microwave irradiation; Sealed tube;