Technology Process of Vinthionine
There total 3 articles about Vinthionine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-amino-4-mercaptobutyric acid;
With
ammonia; sodium;
for 0.166667h;
Sealed tube;
Inert atmosphere;
Cooling with ethanol-dry ice;
acetylene;
In
dimethyl sulfoxide;
at 0 - 20 ℃;
for 4h;
- Guidance literature:
-
DL-homocystine;
With
ammonia; sodium;
at -78 ℃;
for 0.166667h;
acetylene;
In
dimethyl sulfoxide;
at 0 - 20 ℃;
for 4h;
DOI:10.1021/jacs.5b05950
- Guidance literature:
-
In
dimethyl sulfoxide;
at 0 - 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1039/c6ob01690a
