(1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:(1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate)
CAS No.:54535-06-7
Molecular Formula:C24H26O8S2
Molecular Weight:506.598
Hs Code.:
DSSTox Substance ID:DTXSID60389065
Nikkaji Number:J1.145.170E
Wikidata:Q82184459

Synonyms:54535-06-7;(1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate);(1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl)bis(4-methylbenzenesulfonate);ST50299013;DTXSID60389065;1,2-bis(2-tosyloxyethoxy)benzene;1,2-Bis[2-(tosyloxy)ethoxy]benzene;AKOS002313054;A913739;2-(2-{2-[(4-methylbenzenesulfonyl)oxy]ethoxy}phenoxy)ethyl 4-methylbenzene-1-sulfonate

Suppliers and Price of (1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of (1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate)

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:12
Exact Mass:506.10691013
Heavy Atom Count:34
Complexity:718

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OCCOC2=CC=CC=C2OCCOS(=O)(=O)C3=CC=C(C=C3)C

Technology Process of (1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate)

There total 7 articles about (1,2-Phenylenebis(oxy))bis(ethane-2,1-diyl) bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 10234-40-9
2,2'-(1,2-phenylenedioxy)diethanol

: 98-59-9
p-toluenesulfonyl chloride

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/cmdc.201000097

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / piperidine hydrochloride / methanol / 10 h / 40 °C

2: 96 percent / pyridine / -10 - 4 °C

With pyridine; piperidine hydrochloride; In methanol;

Reference yield:

: 52376-09-7
ethyl 2-<2-<(ethoxycarbonyl)methoxy>phenoxy>acetate

bis(o-phenylene)glycol ditosylate: 54535-06-7
bis(o-phenylene)glycol ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

2: 80 percent / pyridine / 4 h / 10 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jm00358a025