(E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde

Base Information

Chemical Name:(E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde
CAS No.:53341-46-1
Molecular Formula:C₁₂H₁₅NO₂
Molecular Weight:205.257
Hs Code.:
Mol file:53341-46-1.mol

Synonyms:100569;(E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde

Suppliers and Price of (E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
(E)-3-(Dimethylamino)-2-(m-tolyloxy)acrylaldehyde 95%
5g
$ 1480.00

Matrix Scientific
(E)-3-(Dimethylamino)-2-(m-tolyloxy)acrylaldehyde 95%
1g
$ 556.00

Total 5 raw suppliers

Chemical Property of (E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

(E)-3-(Dimethylamino)-2-(m-tolyloxy)acrylaldehyde 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde

There total 4 articles about (E)-3-(diMethylaMino)-2-(M-tolyloxy)acrylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(2,2-dimethoxyethoxyl)-3-methylbenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 53341-46-1
(E)-3-(dimethylamino)-2-(meta-tolyloxy)acrylaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; In chloroform; at 30 - 55 ℃; for 2h; Industrial scale;

1-(2,2-dimethoxyethoxyl)-3-methylbenzene; In chloroform; for 2h; Reflux; Industrial scale;

Reference yield:

: 108-39-4
3-methyl-phenol

: 53341-46-1
(E)-3-(dimethylamino)-2-(meta-tolyloxy)acrylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; potassium hydroxide / toluene / 28 h / Reflux; Industrial scale

2.1: trichlorophosphate / chloroform / 2 h / 30 - 55 °C / Industrial scale

2.2: 2 h / Reflux; Industrial scale

With tetrabutylammomium bromide; potassium hydroxide; trichlorophosphate; In chloroform; toluene;

Reference yield:

: 108-39-4
3-methyl-phenol

: 53341-46-1
(E)-3-(dimethylamino)-2-(meta-tolyloxy)acrylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KOH / 1.) H₂O, 90 to 100 deg C, 2.) reflux, 6 h

2: 1.) POCl₃ / 1.) 50 deg C, 45 min, 2.) CHCl₃, reflux, 3 h

With potassium hydroxide; trichlorophosphate;
DOI:10.1021/jm00183a012