Benzenemethanol, 2-bromo-a-ethyl-, (aR)-

Base Information

Chemical Name:Benzenemethanol, 2-bromo-a-ethyl-, (aR)-
CAS No.:157563-40-1
Molecular Formula:C9H11BrO
Molecular Weight:215.09
Hs Code.:
Mol file:157563-40-1.mol

Synonyms:1-(2-bromophenyl)-1-propanol;1-(2-bromophenyl)propan-1-ol;(R)-1-(2-bromophenyl)-1-propanol;(R)-1-(o-bromophenyl)-1-propanol;(R)-1-(2'-bromophenyl)-1-propanol;(R)-1-(2-bromophenyl)propan-1-ol;(R)-1-(2-Bromo-phenyl)-propan-1-ol;

Suppliers and Price of Benzenemethanol, 2-bromo-a-ethyl-, (aR)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzenemethanol, 2-bromo-a-ethyl-, (aR)-

Chemical Property:

PSA：20.23000
LogP:2.89250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenemethanol, 2-bromo-a-ethyl-, (aR)-

There total 4 articles about Benzenemethanol, 2-bromo-a-ethyl-, (aR)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 557-20-0
diethylzinc

: 6630-33-7
ortho-bromobenzaldehyde

: 157563-40-1
(1R)-1-(2-bromophenyl)propan-1-ol

Guidance literature:: diethylzinc; ortho-bromobenzaldehyde; With (2R,3S,3aS,4aR,6R,8aS)-2-isopropyl-6,9,9-trimethyl-3-phenyldecahydro-4aH-pyrrolo[2,1-b][1,3]benzoxazin-3-ol; In hexane; toluene; at 20 ℃; Inert atmosphere;

With ammonium chloride; In hexane; water; toluene; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tetasy.2010.07.016

Reference yield:

: 557-20-0
diethylzinc

: 6630-33-7
ortho-bromobenzaldehyde

: 157563-40-1
(1R)-1-(2-bromophenyl)propan-1-ol

: 170379-92-7
(1S)-1-(2-bromophenyl)propan-1-ol

Guidance literature:: With titanium-(S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol; Multistep reaction. Title compound not separated from byproducts; 1.) CH₂Cl₂, hexane, RT, 10 min, 2.) CH₂Cl₂, hexane, 0 deg C, 5 h;
DOI:10.1016/S0957-4166(97)00501-6