1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate

Base Information

Chemical Name:1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate
CAS No.:912444-87-2
Molecular Formula:C14H25NO5
Molecular Weight:287.35
Hs Code.:2933990090
Mol file:912444-87-2.mol

Synonyms:1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate;Hexahydro-5-hydroxy-1H-azepine-1,4-dicarboxylic acid 1-(tert-butyl) 4-ethyl ester

Suppliers and Price of 1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-tert-Butyl4-ethyl5-hydroxyazepane-1,4-dicarboxylate 95+%
1g
$ 762.00

Chemenu
1-(tert-butyl)4-ethyl5-hydroxyazepane-1,4-dicarboxylate 95%
1g
$ 720.00

Alichem
1-tert-Butyl4-ethyl5-hydroxyazepane-1,4-dicarboxylate
1g
$ 626.20

Abosyn
1-tert-butyl4-ethyl5-hydroxyazepane-1,4-dicarboxylate 95%-98%
1g
$ 540.00

Total 10 raw suppliers

Chemical Property of 1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:382.92°C at 760 mmHg
Flash Point:185.383°C
PSA：76.07000
Density:1.133
LogP:1.49540
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-tert-Butyl4-ethyl5-hydroxyazepane-1,4-dicarboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate

There total 2 articles about 1-tert-Butyl 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 141642-82-2
5-oxo-azepane-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester

: 912444-87-2
1-(tert-butyl) 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 1h;

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 912444-87-2
1-(tert-butyl) 4-ethyl 5-hydroxyazepane-1,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / diethyl ether / 1 h / -78 °C / Inert atmosphere

2: sodium tetrahydroborate; methanol / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether;