AEEA-AEEA

Base Information

• Chemical Name: AEEA-AEEA
• CAS No.: 1143516-05-5
• Molecular Formula: C12H24N2O7
• Molecular Weight: 308.332
• Hs Code.: 2924190090
• Mol file: 1143516-05-5.mol

Synonyms:H-AEEA-AEEA-OH;AEEA-AEEA-AEEA;17-Amino-10-oxo-3,6,12,15-tetraoxa-9-azaheptadecanoic acid;17-amino-10-oxo-3,6,12,15-tetraoxa-9-azaheptadecan-1-oic acid;H-AEEA-AEEA;AEEA-AEEA-OH;AEEA-AEEA;H-Ado-Ado-OH;H-Adoa-Adoa-OH;H2N-PEG2-CH2CONH-PEG2-CH2COOH

Chemical Property of AEEA-AEEA

Chemical Property:

• Boiling Point: 548.7±50.0 °C(Predicted)
• PKA: 3.39±0.10(Predicted)
• PSA: 129.34000
• Density: 1.202±0.06 g/cm3(Predicted)
• LogP: -0.69650
• Storage Temp.: -20°C Freezer, Under inert atmosphere
• Solubility.: DMSO (Slightly, Heated, Sonicated), Methanol (Slightly)

Purity/Quality:

99%, ^*data from raw suppliers

17-Amino-10-oxo-3,6,12,15-tetraoxa-9-azaheptadecanoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 17-Amino-10-oxo-3,6,12,15-tetraoxa-9-azaheptadecanoic Acid is used for preparation of glutamic acid-containing acylating reagents for selective acylation of amino group(s) in peptides or proteins.

Technology Process of AEEA-AEEA

There total 1 articles about AEEA-AEEA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-4,13-dioxo-3,8,11,17,20-pentaoxa-5,14-diazadocosan-22-oic acid (1069067-08-8) → [2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-acetylamino}-ethoxy)-ethoxy]-acetic acid (1143516-05-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 4 - 20 ℃;

DOI:10.1039/c0ob00133c

Reference yield: 96.25%

[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-acetylamino}-ethoxy)-ethoxy]-acetic acid (1143516-05-5) + C41H56N2O9 → (S)-22-((benzyloxy)carbonyl)-3,20,25,34-tetraoxo-1-phenyl-2,29,32,38,41-pentaoxa-21,26,35-triazatritetracontan-43-oic acid

Guidance literature:

With triethylamine; In tetrahydrofuran; at 25 ℃; for 8h; Solvent; Reagent/catalyst; Temperature;

Reference yield: 56.0%

[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-acetylamino}-ethoxy)-ethoxy]-acetic acid (1143516-05-5) + 3-[[5-[[4-[4-(14-tert-butoxy-14-oxotetradecyl)phenoxy]phenyl]sulfonylamino]pyrimidine-2-carbonyl]amino]propanoic acid → 2-[2-[2-[[2-[2-[2-[3-[[5-[[4-[4-(14-tert-butoxy-14-oxotetradecyl)phenoxy]phenyl]sulfonyl amino]pyrimidine-2-carbonyl]-amino]propanoylamino]ethoxy]ethoxy]acetyl]amino]ethoxy]ethoxy]acetic acid

Guidance literature:

3-[[5-[[4-[4-(14-tert-butoxy-14-oxotetradecyl)phenoxy]phenyl]sulfonylamino]pyrimidine-2-carbonyl]amino]propanoic acid; With O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 2h;

[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-acetylamino}-ethoxy)-ethoxy]-acetic acid; In ethanol; at 20 ℃; for 16h;

upstream raw materials:

2,2-dimethyl-4,13-dioxo-3,8,11,17,20-pentaoxa-5,14-diazadocosan-22-oic acid

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