Technology Process of 2-Methoxy-6-(methylsulfonyl)aniline
There total 6 articles about 2-Methoxy-6-(methylsulfonyl)aniline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 1h;
under 760 Torr;
DOI:10.1021/jm00063a014
- Guidance literature:
-
Multi-step reaction with 6 steps
1: SOCl2
2: 1.) NaN3, 2.) H2O, 4.) NaOH, 5.) HCl
3: 1.) 98percent sulfuric acid, NaNO2, 2.) CuCl2, 36percent aq. HCl / 1.) acetic acid, 10 deg C, 1 h, 2.) acetic acid, RT, 1 h
4: 35 percent / dimethylformamide; H2O / 2 h / 100 °C
5: 61 percent / mcpba / CH2Cl2 / Ambient temperature
6: 99 percent / H2 / 10percent Pd/C / ethyl acetate / 1 h / 760 Torr
With
hydrogenchloride; sodium hydroxide; thionyl chloride; sodium azide; sulfuric acid; water; hydrogen; 3-chloro-benzenecarboperoxoic acid; copper dichloride; sodium nitrite;
palladium on activated charcoal;
In
dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00063a014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 35 percent / dimethylformamide; H2O / 2 h / 100 °C
2: 61 percent / mcpba / CH2Cl2 / Ambient temperature
3: 99 percent / H2 / 10percent Pd/C / ethyl acetate / 1 h / 760 Torr
With
hydrogen; 3-chloro-benzenecarboperoxoic acid;
palladium on activated charcoal;
In
dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00063a014