N-(CyclohexylMethyl)-n-MethylaMine, HCl

Base Information

• Chemical Name: N-(CyclohexylMethyl)-n-MethylaMine, HCl
• CAS No.: 161353-93-1
• Molecular Formula: C8H17N.ClH
• Molecular Weight: 163.68822
• Mol file: 161353-93-1.mol

Synonyms:(cyclohexylmethyl)methylamine HCL;N-(CyclohexylMethyl)-n-MethylaMine, HCl;(cyclohexylMethyl)MethylaMine hydrochloride;Cyclohexanemethanamine, N-methyl-, hydrochloride (1:1)

Chemical Property of N-(CyclohexylMethyl)-n-MethylaMine, HCl

Chemical Property:

Purity/Quality:

≥95% ^*data from raw suppliers

N-(Cyclohexylmethyl)-N-methylamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(CyclohexylMethyl)-n-MethylaMine, HCl

There total 3 articles about N-(CyclohexylMethyl)-n-MethylaMine, HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl N-(cyclohexylmethyl)-N-methylcarbamate (1239325-65-5) → 1-cyclohexyl-N-methylmethanamine hydrochloride (161353-93-1)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 1.5h;

Reference yield:

cyclohexylmethylamine (3218-02-8) → 1-cyclohexyl-N-methylmethanamine hydrochloride (161353-93-1)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 1 h / Cooling with ice

2: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Cooling with ice

3: hydrogenchloride / ethyl acetate / 1.5 h / 20 °C

With hydrogenchloride; sodium hydride; triethylamine; In tetrahydrofuran; ethyl acetate; mineral oil;

Reference yield:

tert-butyl N-cyclohexylmethylcarbamate (56700-67-5) → 1-cyclohexyl-N-methylmethanamine hydrochloride (161353-93-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Cooling with ice

2: hydrogenchloride / ethyl acetate / 1.5 h / 20 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; ethyl acetate; mineral oil;

upstream raw materials:

cyclohexylmethylamine

tert-butyl N-cyclohexylmethylcarbamate

tert-butyl N-(cyclohexylmethyl)-N-methylcarbamate

Refernces