1,3,5,7-tetrakis(4-aminophenyl)adamantane

Base Information

Chemical Name:1,3,5,7-tetrakis(4-aminophenyl)adamantane
CAS No.:158562-40-4
Molecular Formula:C34H36N4
Molecular Weight:500.68
Hs Code.:
Mol file:158562-40-4.mol

Synonyms:Benzenamine, 4,4',4'',4'''-tricyclo[3.3.1.13,7]decane-1,3,5,7-tetrayltetrakis-;4,4',4'',4'''-Tricyclo[3.3.1.13,7]decane-1,3,5,7-tetrayltetrakis[benzenamine];

Suppliers and Price of 1,3,5,7-tetrakis(4-aminophenyl)adamantane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
4,4,4,4-Tricyclo[3.3.1.1]decane-1,3,5,7-tetrayltetrakis[benzenamine] 98%
1g
$ 456.00

Total 9 raw suppliers

Chemical Property of 1,3,5,7-tetrakis(4-aminophenyl)adamantane

Chemical Property:

Melting Point:404 °C
Boiling Point:737.8±60.0 °C(Predicted)
PKA:5.39±0.10(Predicted)
PSA：104.08000
Density:1.302±0.06 g/cm3(Predicted)
LogP:8.77340

Purity/Quality:

97% ^*data from raw suppliers

4,4,4,4-Tricyclo[3.3.1.1]decane-1,3,5,7-tetrayltetrakis[benzenamine] 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3,5,7-tetrakis(4-aminophenyl)adamantane

There total 5 articles about 1,3,5,7-tetrakis(4-aminophenyl)adamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 167013-18-5
1,3,5,7-tetrakis-(4-nitrophenyl)adamantane

: 158562-40-4
1,3,5,7-tetrakis-(4-aminophenyl)adamantane

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; under 760.051 Torr; Inert atmosphere;
DOI:10.1039/b912189g

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 158562-40-4
1,3,5,7-tetrakis-(4-aminophenyl)adamantane

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride; t-butyl bromide / 7 h / Inert atmosphere; Cooling with ice; Reflux

2.1: nitric acid / 2 h / -18 - -10 °C

2.2: 0.25 h / -10 °C

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 20 °C

With aluminum (III) chloride; t-butyl bromide; palladium 10% on activated carbon; hydrogen; nitric acid; In tetrahydrofuran;
DOI:10.1039/c6ta01457g

Reference yield:

: 768-90-1
1-Adamantyl bromide

: 158562-40-4
1,3,5,7-tetrakis-(4-aminophenyl)adamantane

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride; t-butyl bromide / 7 h / Inert atmosphere; Cooling with ice; Reflux

2.1: nitric acid / 2 h / -18 - -10 °C

2.2: 0.25 h / -10 °C

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 20 °C

With aluminum (III) chloride; t-butyl bromide; palladium 10% on activated carbon; hydrogen; nitric acid; In tetrahydrofuran;
DOI:10.1039/c6ta01457g