Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrakis(4-bromophenyl)-

Base Information

• Chemical Name: Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrakis(4-bromophenyl)-
• CAS No.: 144970-36-5
• Molecular Formula: C34H28Br4
• Molecular Weight: 756.212
• Mol file: 144970-36-5.mol

Synonyms:Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrakis(4-bromophenyl)-

Chemical Property of Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrakis(4-bromophenyl)-

Chemical Property:

• Boiling Point: 683.6±55.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.718±0.06 g/cm3(Predicted)
• LogP: 11.16980

Purity/Quality:

≥99% ^*data from raw suppliers

1,3,5,7-Tetrakis(4-bromophenyl)adamantane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrakis(4-bromophenyl)-

There total 2 articles about Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrakis(4-bromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,3,5,7-tetrakis(phenyl)adamantane (16004-75-4) → 1,3,5,7-tetrakis(4-bromophenyl)adamantane (144970-36-5)

Guidance literature:

With bromine; iron; In chloroform; at 45 - 50 ℃;

DOI:10.1080/00304940409458678

Reference yield:

→ 1,3,5,7-tetrakis(4-bromophenyl)adamantane (144970-36-5)

Guidance literature:

Reference yield: 76.0%

4-methoxycarbonylphenylboronic acid (99768-12-4) + 1,3,5,7-tetrakis(4-bromophenyl)adamantane (144970-36-5) → C66H56O8

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; In 1,2-dimethoxyethane; for 48h; Inert atmosphere; Reflux; Schlenk technique;

upstream raw materials:

1,3,5,7-tetrakis(phenyl)adamantane

Downstream raw materials:

1,3,5,7-tetrakis-(4-cyanophenyl)adamantane

((adamantane-1,3,5,7-tetrayl)tetra(phen-4- yl))tetracarboxylic acid

1,3,5,7-tetrakis(4-methoxyphenyl)adamantane