4-BROMO-1-BUTANOL

Base Information

• Chemical Name: 4-BROMO-1-BUTANOL
• CAS No.: 6089-17-4
• Molecular Formula: C4H9BrO
• Molecular Weight: 153.019
• Hs Code.: 2905590090
• Mol file: 6089-17-4.mol

Synonyms:1-Bromo-3-butanol;4-Bromobutan-2-ol;

Chemical Property of 4-BROMO-1-BUTANOL

Chemical Property:

• Boiling Point: 184.559 °C at 760 mmHg
• PKA: 14.72±0.20(Predicted)
• Flash Point: 85.508 °C
• PSA: 20.23000
• Density: 1.449 g/cm³
• LogP: 1.15380
• Storage Temp.: −20°C

Purity/Quality:

98%Min ^*data from raw suppliers

4-Bromo-1-butanol, 97% 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F,Xi
• Hazard Codes: F,Xi
• Statements: 11-36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BROMO-1-BUTANOL

There total 1 articles about 4-BROMO-1-BUTANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1.3-butanediol (18826-95-4,107-88-0) → 4-bromobutan-2-ol (6089-17-4) + 3-bromo-1-butanol (6089-12-9)

Guidance literature:

With 3-ethyl-2-chlorobenzoxazolium tetrafluoroborate; tetrabutylammomium bromide; In acetonitrile; at 25 ℃;

DOI:10.1021/acscatal.1c04239

Reference yield: 83.0%

4-bromobutan-2-ol (6089-17-4) + N6-benzyloxy-9-(diphenylmethyl)adenine (608523-19-9) → N6-benzyloxy-7-(3-hydroxybutyl)-9-(diphenylmethyl)adeninium bromide

Guidance literature:

In N,N-dimethyl-formamide; at 70 ℃; for 72h;

DOI:10.1016/S0040-4020(03)01058-5

Reference yield: 82.0%

4-bromobutan-2-ol (6089-17-4) + (E)-1,2-bis(phenylsulfonyl)ethylene (963-16-6) → [(E)-2-(3-Bromo-1-methyl-propoxy)-ethenesulfonyl]-benzene (199862-39-0)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1021/jo991970b

upstream raw materials:

1.3-butanediol

Downstream raw materials:

Dimethyl-thiophosphoramidic acid S-(3-hydroxy-butyl) ester O-phenyl ester

[(E)-2-(3-Bromo-1-methyl-propoxy)-ethenesulfonyl]-benzene

benzyl-(3-bromo-1-methyl-propyl)-ether

1-(3-bromo-1-methylpropyl)-3-(2-fluorophenyl)-1,3-dihydro-2,1,3-benzothiadiazole 2,2-dioxide

Refernces