5-Ethylindoline

Base Information

Chemical Name:5-Ethylindoline
CAS No.:67932-65-4
Molecular Formula:C10H13N
Molecular Weight:147.21700
Hs Code.:2933990090
European Community (EC) Number:857-363-0
DSSTox Substance ID:DTXSID60588511
Wikidata:Q82481219
Mol file:67932-65-4.mol

Synonyms:5-Ethylindoline;67932-65-4;5-ethyl-2,3-dihydro-1H-indole;1H-INDOLE,5-ETHYL-2,3-DIHYDRO-;SCHEMBL395752;DTXSID60588511;DWLKQZKMPDGRNB-UHFFFAOYSA-N;AKOS009133036;MCULE-7733620345;SB65397;CS-0252039;EN300-57712

Suppliers and Price of 5-Ethylindoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
1H-INDOLE,5-ETHYL-2,3-DIHYDRO- 95
10g
$ 2198.00

Labseeker
1H-INDOLE,5-ETHYL-2,3-DIHYDRO- 95
1g
$ 1267.00

Crysdot
5-Ethylindoline 95+%
1g
$ 491.00

Chemenu
5-ethylindoline 95%
1g
$ 464.00

American Custom Chemicals Corporation
1H-INDOLE,5-ETHYL-2,3-DIHYDRO- 95.00%
5MG
$ 505.80

Alichem
5-Ethylindoline
1g
$ 429.07

AK Scientific
5-Ethylindoline
10g
$ 4436.00

AK Scientific
5-Ethylindoline
5g
$ 3032.00

AK Scientific
5-Ethylindoline
2.5g
$ 2092.00

AK Scientific
5-Ethylindoline
500mg
$ 910.00

Total 4 raw suppliers

Chemical Property of 5-Ethylindoline

Chemical Property:

Vapor Pressure:0.018mmHg at 25°C
Boiling Point:253.7oC at 760 mmHg
PKA:5.83±0.20(Predicted)
Flash Point:111.1oC
PSA：12.03000
Density:0.998g/cm3
LogP:2.35500
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:147.104799419
Heavy Atom Count:11
Complexity:133

Purity/Quality:

99% ^*data from raw suppliers

1H-INDOLE,5-ETHYL-2,3-DIHYDRO- 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=CC2=C(C=C1)NCC2

Technology Process of 5-Ethylindoline

There total 7 articles about 5-Ethylindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 118757-02-1
1-benzenesulfonyl-5-ethyl-2,3-dihydro-1H-indole

: 67932-65-4
5-ethyl-2,3-dihydro-1H-indole

Guidance literature:: 1-benzenesulfonyl-5-ethyl-2,3-dihydro-1H-indole; With hydrogen bromide; In water; for 6h; Heating / reflux;

With sodium hydroxide; In water; pH=9;

Reference yield:

: 496-15-1
1-indoline

: 67932-65-4
5-ethyl-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane / 20 °C / Cooling with ice-water bath

2.1: aluminum (III) chloride / dichloromethane / 0.25 h

2.2: 5 h

3.1: trifluoroacetic acid; sodium tetrahydroborate / 0 - 25 °C

4.1: water; hydrogen bromide / 6 h / Reflux

4.2: pH 9

With dmap; aluminum (III) chloride; sodium tetrahydroborate; water; hydrogen bromide; triethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 81114-41-2
1-benzenesulfonyl-2,3-dihydro-1H-indole

: 67932-65-4
5-ethyl-2,3-dihydro-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 0.25 h

1.2: 5 h

2.1: trifluoroacetic acid; sodium tetrahydroborate / 0 - 25 °C

3.1: water; hydrogen bromide / 6 h / Reflux

3.2: pH 9

With aluminum (III) chloride; sodium tetrahydroborate; water; hydrogen bromide; trifluoroacetic acid; In dichloromethane;