(2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER

Base Information

Chemical Name:(2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER
CAS No.:579474-49-0
Molecular Formula:C11H15ClN2O2
Molecular Weight:242.705
Hs Code.:
Mol file:579474-49-0.mol

Synonyms:(2-amino-4-chloro-phenyl)-carbamic acid tert-butyl ester;(2-amino-4-chloro-phenyl)carbamic acid tert-butyl ester;

Suppliers and Price of (2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(2-amino-4-chlorophenyl)carbamate 95+%
1g
$ 339.00

American Custom Chemicals Corporation
(2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER 96.00%
5MG
$ 505.02

Alichem
tert-Butyl(2-amino-4-chlorophenyl)carbamate
1g
$ 287.04

Acrotein
tert-Butyl(2-amino-4-chlorophenyl)carbamate 97%
1g
$ 388.71

Acrotein
tert-Butyl(2-amino-4-chlorophenyl)carbamate 97%
0.25g
$ 158.33

Total 8 raw suppliers

Chemical Property of (2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER

Chemical Property:

Boiling Point:312.0±32.0 °C(Predicted)
PKA:12.60±0.70(Predicted)
PSA：64.35000
Density:1.259±0.06 g/cm3(Predicted)
LogP:3.92340

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(2-amino-4-chlorophenyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER

There total 4 articles about (2-AMINO-4-CHLORO-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (4-Chloro-2-nitro-phenyl)-carbamic acid tert-butyl ester

: 579474-49-0
(2-amino-4-chlorophenyl)carbamate tert-butyl ester

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In 1,4-dioxane; water; at 100 ℃; for 0.666667h;
DOI:10.1021/acs.jmedchem.6b00709

Reference yield: 85.0%

: 579474-49-0
(2-amino-4-chlorophenyl)carbamate tert-butyl ester

Guidance literature:: With ferrous(II) sulfate heptahydrate; ammonium chloride; zinc; In ethanol; water; at 20 - 50 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 579474-49-0
(2-amino-4-chlorophenyl)carbamate tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.67 h / 0 - 20 °C

1.2: 15 h / 20 °C

2.1: sodium dithionite; sodium hydrogencarbonate / 1,4-dioxane; water / 0.67 h / 100 °C

With sodium dithionite; sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.6b00709