2-(4-CHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE

Base Information

• Chemical Name: 2-(4-CHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE
• CAS No.: 1221715-46-3
• Molecular Formula: C8H6FN3O2
• Molecular Weight: 195.15100
• Mol file: 1221715-46-3.mol

Synonyms:BENZOIC ACID,3-FLUORO-6-IODO-2-METHYL-,METHYL ESTER;methyl 3-fluoro-D,L-alanine hydrochloride;

Chemical Property of 2-(4-CHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE

Chemical Property:

• PSA: 56.49000
• LogP: 0.65500

Purity/Quality:

98% ^*data from raw suppliers

methyl3-fluoroimidazo[1,2-a]pyrimidine-2-carboxylate 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-CHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE

There total 1 articles about 2-(4-CHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

methyl 2-[(pyrimidin-2-yl)imino]-3,3,3-trifluoropropanoate (1236112-71-2) → methyl 3-fluoroimidazo[1,2-a]pyrimidine-2-carboxylate (1221715-46-3)

Guidance literature:

With triethyl phosphite; In diethyl ether; at 0 - 20 ℃;

DOI:10.1016/j.jfluchem.2010.06.019

Reference yield: 78.0%

methyl 3-fluoroimidazo[1,2-a]pyrimidine-2-carboxylate (1221715-46-3) + benzylamine (100-46-9) → methyl 3-benzylaminoimidazo[1,2-a]pyrimidine-2-carboxylate (1236112-74-5)

Guidance literature:

In acetonitrile; for 1h; Reflux;

DOI:10.1007/s11172-009-0198-9

upstream raw materials:

methyl 2-[(pyrimidin-2-yl)imino]-3,3,3-trifluoropropanoate

Downstream raw materials:

methyl 3-benzylaminoimidazo[1,2-a]pyrimidine-2-carboxylate

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