1H-Isoindol-1-one, 2,3-dihydro-6-methoxy-7-methyl-

Base Information

• Chemical Name: 1H-Isoindol-1-one, 2,3-dihydro-6-methoxy-7-methyl-
• CAS No.: 1138220-74-2
• Molecular Formula: C10H11NO2
• Molecular Weight: 177.20000
• Hs Code.: 2933790090
• Mol file: 1138220-74-2.mol

Synonyms:6-Methoxy-7-methyl-3-(1H-tetrazol-5-yl)coumarin;6-Methoxy-7-methyl-2H-1-benzopyran-2-one;6-methoxy-7-methylisoindolin-1one;2H-1-Benzopyran-2-one,6-methoxy-7-methyl;

Chemical Property of 1H-Isoindol-1-one, 2,3-dihydro-6-methoxy-7-methyl-

Chemical Property:

• PSA: 38.33000
• LogP: 1.57580

Purity/Quality:

98%min ^*data from raw suppliers

6-Methoxy-7-methyl-2,3-dihydro-1H-isoindol-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1H-Isoindol-1-one, 2,3-dihydro-6-methoxy-7-methyl-

There total 1 articles about 1H-Isoindol-1-one, 2,3-dihydro-6-methoxy-7-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methyl 6-cyano-3-methoxy-2-methylbenzoate (55289-18-4) → 6-methoxy-7-methylisoindolin-1one (1138220-74-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; for 72h; under 2844.39 Torr;

DOI:10.1016/j.tetlet.2008.12.099

Reference yield: 94.0%

6-methoxy-7-methylisoindolin-1one (1138220-74-2) → 6-hydroxy-7-methylisoindolin-1one (1138220-70-8)

Guidance literature:

With boron tribromide; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1016/j.tetlet.2008.12.099

upstream raw materials:

methyl 6-cyano-3-methoxy-2-methylbenzoate

Downstream raw materials:

6-hydroxy-7-methylisoindolin-1one

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