BUTTPARK 120\07-93

Base Information

• Chemical Name: BUTTPARK 120\07-93
• CAS No.: 874841-30-2
• Molecular Formula: C14H16N2O2
• Molecular Weight: 244.28900
• Mol file: 874841-30-2.mol

Synonyms:

Chemical Property of BUTTPARK 120\07-93

Chemical Property:

• PSA: 53.33000
• LogP: 2.92088

Purity/Quality:

98%+ ^*data from raw suppliers

TERT-BUTYL-5-CYANOINDOLINE-1-CARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BUTTPARK 120\07-93

There total 3 articles about BUTTPARK 120\07-93 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

potassium hexacyanoferrate(II) trihydrate + 1-(tert-butoxycarbonyl)-5-chloroindoline (143262-12-8) → tert-butyl 5-cyanoindoline-1-carboxylate (874841-30-2)

Guidance literature:

With C₃₆H₅₅ClPPd; potassium acetate; In 1,4-dioxane; water; at 90 ℃; for 1.33333h; Sealed tube;

DOI:10.1021/acs.joc.8b00515

Reference yield: 93.0%

tert-butyl 5-bromoindoline-1-carboxylate (261732-38-1) + potassium hexacyanoferrate(II) trihydrate → tert-butyl 5-cyanoindoline-1-carboxylate (874841-30-2)

Guidance literature:

With C₃₆H₅₅ClPPd; potassium acetate; In 1,4-dioxane; water; at 90 ℃; for 1.33333h; Reagent/catalyst; Sealed tube;

DOI:10.1021/acs.joc.8b00515

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + indoline-5-carbonitrile (15861-23-1) → tert-butyl 5-cyanoindoline-1-carboxylate (874841-30-2)

Guidance literature:

In tetrahydrofuran;

DOI:10.1016/j.bmcl.2011.05.110

upstream raw materials:

di-tert-butyl dicarbonate

indoline-5-carbonitrile

1-(tert-butoxycarbonyl)-5-chloroindoline

tert-butyl 5-bromoindoline-1-carboxylate

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