p-Methacryloyloxybenzoic acid

Base Information

• Chemical Name: p-Methacryloyloxybenzoic acid
• CAS No.: 15721-10-5
• Molecular Formula: C11H10 O4
• Molecular Weight: 206.198
• Hs Code.: 2918990090
• Mol file: 15721-10-5.mol

Synonyms:Benzoicacid, 4-[(2-methyl-1-oxo-2-propenyl)oxy]- (9CI); Benzoic acid, p-hydroxy-,methacrylate (8CI); Methacrylic acid, ester with p-hydroxybenzoic acid;Methacrylic acid, p-hydroxybenzoate (8CI); 4-Carboxyphenyl methacrylate;4-Methacryloyloxybenzoic acid; p-(Methacryloyloxy)benzoic acid

Chemical Property of p-Methacryloyloxybenzoic acid

Chemical Property:

• Vapor Pressure: 3.47E-06mmHg at 25°C
• Boiling Point: 371.8°Cat760mmHg
• Flash Point: 147.3°C
• PSA: 63.60000
• Density: 1.23g/cm³
• LogP: 1.86630

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-Methacryloyloxybenzoic acid

There total 3 articles about p-Methacryloyloxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

→ 4-methacryloyloxybenzoic acid (15721-10-5)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 5.5h;

Reference yield:

methacryloyl anhydride (760-93-0) + 4-hydroxy-benzoic acid (99-96-7) → 4-methacryloyloxybenzoic acid (15721-10-5)

Guidance literature:

at 60 ℃; for 1h; Cooling with ice;

Reference yield:

Methacryloyl chloride (920-46-7,26937-45-1) + 4-hydroxy-benzoic acid (99-96-7) → 4-methacryloyloxybenzoic acid (15721-10-5)

Guidance literature:

With sodium hydroxide; for 2h; Yield given; Ambient temperature; pH 10-11;

upstream raw materials:

Methacryloyl chloride

4-hydroxy-benzoic acid

methacryloyl anhydride

Downstream raw materials:

p-methacryloyloxybenzoyl chloride

Refernces

• 1、 ?etin, Sedat,?ztürk ?en, Behiye,Soykan, U?ur,Firat, Elif Esra,Yildirim, Gürcan. "Experimental and theoretical approaches for structural and mechanical properties of novel side chain LCP-PP graft coproducts". . p. 467 - 483. Retrieved 2016/07/06.
• 2、 Zhou, Qingzhong,Huang, Zhen. "Immobilized thermolysin and synthesis of precursor of aspartame". . p. 35 - 39. Retrieved 2007/10/02.