3,8-Dimethylimidazo[1,2-A]pyridine

Base Information

• Chemical Name: 3,8-Dimethylimidazo[1,2-A]pyridine
• CAS No.: 1284210-50-9
• Molecular Formula: C9H10N2
• Molecular Weight: 146.18900
• DSSTox Substance ID: DTXSID20706436
• Nikkaji Number: J3.165.554D
• Wikidata: Q82639798

Synonyms:3,8-DIMETHYLIMIDAZO[1,2-A]PYRIDINE;1284210-50-9;SCHEMBL13556610;DTXSID20706436;AKOS018443714;imidazo[1,2-a]pyridine,3,8-dimethyl-

Chemical Property of 3,8-Dimethylimidazo[1,2-A]pyridine

Chemical Property:

• PSA: 17.30000
• LogP: 1.95110
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 146.084398327
• Heavy Atom Count: 11
• Complexity: 147

Purity/Quality:

98% ^*data from raw suppliers

3,8-Dimethylimidazo[1,2-a]pyridine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=CN2C1=NC=C2C

Technology Process of 3,8-Dimethylimidazo[1,2-A]pyridine

There total 3 articles about 3,8-Dimethylimidazo[1,2-A]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-(tert-butoxycarbonyl)-N-[2-(3-methylpyridyl)]-3-amino-1-propyne → 3,8-dimethylimidazo[1,2-a]pyridine (1284210-50-9)

Guidance literature:

With water; at 120 ℃; for 1.5h; Inert atmosphere; Sealed tube;

DOI:10.1016/j.tetlet.2013.08.112

Reference yield: 80.0%

3-methyl-N-(prop-2-yn-1-yl)pyridin-2-amine (1250146-65-6) → 3,8-dimethylimidazo[1,2-a]pyridine (1284210-50-9)

Guidance literature:

In water; at 120 ℃; for 1h; Inert atmosphere; Sealed tube;

DOI:10.1021/jo3025303

Reference yield: 67.0%

3-methyl-N-(prop-2-yn-1-yl)pyridin-2-amine (1250146-65-6) → 3,8-dimethylimidazo[1,2-a]pyridine (1284210-50-9) + 8-methylimidazo<1,2-a>pyridine-3-carboxaldehyde (175878-16-7)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; oxygen; silver nitrate; In acetonitrile; at 60 ℃; for 2h;

DOI:10.1021/jo3025303

upstream raw materials:

3-methyl-N-(prop-2-yn-1-yl)pyridin-2-amine

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