1H-BenziMidazole-1-carboxylicacid,6-(broMoMethyl)-,1,1-diMethylethylester

Base Information

• Chemical Name: 1H-BenziMidazole-1-carboxylicacid,6-(broMoMethyl)-,1,1-diMethylethylester
• CAS No.: 226250-03-9
• Molecular Formula: C13H15BrN2O2
• Molecular Weight: 311.17400
• Mol file: 226250-03-9.mol

Synonyms:tert-Butyl 6-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate;

Chemical Property of 1H-BenziMidazole-1-carboxylicacid,6-(broMoMethyl)-,1,1-diMethylethylester

Chemical Property:

• PSA: 44.12000
• LogP: 3.71440
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

≥99% ^*data from raw suppliers

tert-Butyl6-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-BenziMidazole-1-carboxylicacid,6-(broMoMethyl)-,1,1-diMethylethylester

There total 2 articles about 1H-BenziMidazole-1-carboxylicacid,6-(broMoMethyl)-,1,1-diMethylethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 6-methyl-1H-benzo[d]imidazole-1-carboxylate (863877-82-1) + tert-butyl 5-methyl-1H-benzo[d]imidazole-1-carboxylate (863877-81-0) → tert-butyl 6-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate (226250-03-9) + tert-butyl 5-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate (1037207-08-1)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 90 ℃; for 12h;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 5-methylbenzimidazole (614-97-1) → tert-butyl 6-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate (226250-03-9) + tert-butyl 5-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate (1037207-08-1)

Guidance literature:

di-tert-butyl dicarbonate; 5-methylbenzimidazole; With triethylamine; In dichloromethane; at 20 ℃;

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; Overall yield = 0.7 g; Reflux; Inert atmosphere;

Reference yield:

(piperidinomethyl)polystyrene + tert-butyl 6-(bromomethyl)-1H-benzo[d]imidazole-1-carboxylate (226250-03-9) + 4-[{N-(2-(tert-butoxycarbonylamino)-5-trifluoromethylbenzoyl)glycyl}aminomethyl]piperidine + phenyl isocyanate (103-71-9) → 4-[{N-(2-Amino-5-trifluoromethylbenzoyl)glycyl}aminomethyl]-1-(benz[d]imidazol-5-yl)piperidine

Guidance literature:

With hydrogenchloride; ammonia; In 1,4-dioxane; methanol; acetonitrile;

upstream raw materials:

tert-butyl 6-methyl-1H-benzo[d]imidazole-1-carboxylate

tert-butyl 5-methyl-1H-benzo[d]imidazole-1-carboxylate

di-tert-butyl dicarbonate

5-methylbenzimidazole

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