3H-Imidazo[4,5-c]pyridin-4-amine, 7-methyl-

Base Information

• Chemical Name: 3H-Imidazo[4,5-c]pyridin-4-amine, 7-methyl-
• CAS No.: 1031750-29-4
• Molecular Weight: 148.17
• Mol file: 1031750-29-4.mol

Synonyms:

Chemical Property of 3H-Imidazo[4,5-c]pyridin-4-amine, 7-methyl-

Chemical Property:

Purity/Quality:

97% purity ^*data from raw suppliers

7-methyl-1H-imidazo[4,5-c]pyridin-4-amine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3H-Imidazo[4,5-c]pyridin-4-amine, 7-methyl-

There total 1 articles about 3H-Imidazo[4,5-c]pyridin-4-amine, 7-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-chloro-7-methyl-1(H)-imidazo[4,5-c]pyridine (18232-95-6) → 3-deaza-3-methyladenine (1031750-29-4)

Guidance literature:

4-chloro-7-methyl-1(H)-imidazo[4,5-c]pyridine; With hydrazine; for 30h; Reflux;

In water; for 3h; Reflux; Inert atmosphere;

DOI:10.1021/ol9025028

Reference yield:

tetramethylsuccinic anhydride (35046-68-5) + 3-deaza-3-methyladenine (1031750-29-4) → N-(7-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-2,2,3,3-tetramethylsuccinimide (1202405-84-2) + C15H20N4O3

Guidance literature:

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; for 18h; Inert atmosphere; Reflux;

DOI:10.1021/ol9025028

Reference yield:

phthalic anhydride (85-44-9) + 3-deaza-3-methyladenine (1031750-29-4) → C15H10N4O2 + C15H12N4O3

Guidance literature:

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; Inert atmosphere; Reflux;

DOI:10.1021/ol9025028

upstream raw materials:

4-chloro-7-methyl-1(H)-imidazo[4,5-c]pyridine

Downstream raw materials:

N-(7-methyl-1H-imidazo[4,5-c]pyridin-4-yl)-2,2,3,3-tetramethylsuccinimide

Refernces