2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride

Base Information

• Chemical Name: 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride
• CAS No.: 5912-19-6
• Molecular Formula: C7H8N2 . ClH
• Molecular Weight: 156.615
• Hs Code.: 2933990090
• Mol file: 5912-19-6.mol

Synonyms:1H-Pyrrolo[3,2-c]pyridine, 2,3-dihydro-, hydrochloride (7CI,8CI);

Chemical Property of 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride

Chemical Property:

• Melting Point: 129-130 °C
• PSA: 24.92000
• LogP: 1.98960
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

2,3-dihydro-1h-pyrrolo[3,2-c]pyridinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,3-Dihydro-1h-pyrrolo[3,2-c] Pyridine Hydrochloride is a reactant or enzyme inhibitor used in synthetic preparation of Heterocyclic compounds.

Technology Process of 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride

There total 1 articles about 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.5%

tert-butyl 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate (219834-81-8) → 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride (5912-19-6)

Guidance literature:

With hydrogenchloride; In dichloromethane; ethyl acetate; at 20 ℃; for 2h;

Reference yield: 45.0%

2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride (5912-19-6) + methyl 4-[2-(4-{[(2-{[3-(chlorosulfonyl)benzoyl]amino}-4,5,6,7-tetrahydro-1-benzothiophen-3-yl)carbonyl]amino}phenyl)ethyl]benzoate (1346136-07-9) → methyl 4-(4-(2-(3-((2,3-dihydro-1H-pyrrolo[3,2-c]pyridin-1-yl)sulfonyl)benzamido)-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl-aminoformyl)phenethyl)benzoate

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

Reference yield: 31.0%

2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride (5912-19-6) → 7-bromo-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine (1198293-24-1)

Guidance literature:

2,3-dihydro-1H-pyrrolo[3,2-c]pyridine hydrochloride; With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃;

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide;

upstream raw materials:

tert-butyl 2,3-dihydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

Downstream raw materials:

7-bromo-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine

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