(3-Methylpyridin-4-yl)MethanaMine dihydrochloride

Base Information

• Chemical Name: (3-Methylpyridin-4-yl)MethanaMine dihydrochloride
• CAS No.: 85127-50-0
• Molecular Formula: C7H10N2 . 2ClH
• Molecular Weight: 195.092
• Hs Code.: 2933399990
• Mol file: 85127-50-0.mol

Synonyms:4-Pyridinemethanamine, 3-methyl-, dihydrochloride (9CI);

Chemical Property of (3-Methylpyridin-4-yl)MethanaMine dihydrochloride

Chemical Property:

• Melting Point: 224 °C (decomp)
• PSA: 38.91000
• LogP: 2.35100

Purity/Quality:

99% ^*data from raw suppliers

[(3-methyl-4-pyridinyl)methyl]aminedihydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-Methylpyridin-4-yl)MethanaMine dihydrochloride

There total 1 articles about (3-Methylpyridin-4-yl)MethanaMine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-[1-Acetyl-3-methyl-1H-pyridin-(4Z)-ylidene]-2-phenyl-4H-oxazol-5-one (85127-47-5) → 1-(3-methylpyridin-4-yl)methanamine dihydrochloride (85127-50-0) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With hydrogenchloride; In water; for 3h; Heating;

Reference yield: 73.0%

5-hydroxy-3-oxo-N-phenyl-3,6-dihydro-2H-pyran-4-carbothioamide + 1-(3-methylpyridin-4-yl)methanamine dihydrochloride (85127-50-0) → 5-{[(3-methylpyridin-4-yl)methyl]amino}-3-oxo-N-phenyl-3,6-dihydro-2H-pyran-4-carbothioamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; at 120 ℃; for 2h;

Reference yield: 55.0%

tert-butyl 5-hydroxy-3-oxo-4-(phenylcarbamothioyl)-3,6-dihydropyridine-1(2H)-carboxylate + 1-(3-methylpyridin-4-yl)methanamine dihydrochloride (85127-50-0) → tert-butyl 5-{[(3-methylpyridin-4-yl)methyl]amino}-3-oxo-4-(phenylcarbamothioyl)-3,6-dihydropyridine-1(2H)-carboxylate

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; at 120 ℃; for 2h;

upstream raw materials:

4-[1-Acetyl-3-methyl-1H-pyridin-(4Z)-ylidene]-2-phenyl-4H-oxazol-5-one

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