3-Heptadecyl-1,2-benzenediol diacetate

Base Information

Chemical Name:3-Heptadecyl-1,2-benzenediol diacetate
CAS No.:76619-72-2
Molecular Formula:C₂₇H₄₄O₄
Molecular Weight:432.644
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Heptadecyl-1,2-benzenediol diacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Heptadecyl-1,2-benzenediol diacetate

There total 8 articles about 3-Heptadecyl-1,2-benzenediol diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5653-67-8
2,3-dimethoxybenzyl alcohol

: 76619-72-2
diacetyl-3-n-heptadecylcatechol

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / PBr₃ / diethyl ether / 2.5 h / Ambient temperature

2: 99 percent / benzene / 5 h / Heating

3: n-BuLi / tetrahydrofuran; hexane / 16 h / Heating

4: H₂ / Pd-C / 2-methyl-propan-2-ol

5: 78 percent / BBr₃ / CH₂Cl₂

6: pyridine / 4 h / Ambient temperature

With n-butyllithium; hydrogen; boron tribromide; phosphorus tribromide; palladium on activated charcoal; In tetrahydrofuran; pyridine; diethyl ether; hexane; dichloromethane; tert-butyl alcohol; benzene;
DOI:10.1002/jps.2600720719

Reference yield:

: 54636-77-0
2,3-dimethoxybenzyl bromide

: 76619-72-2
diacetyl-3-n-heptadecylcatechol

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / benzene / 5 h / Heating

2: n-BuLi / tetrahydrofuran; hexane / 16 h / Heating

3: H₂ / Pd-C / 2-methyl-propan-2-ol

4: 78 percent / BBr₃ / CH₂Cl₂

5: pyridine / 4 h / Ambient temperature

With n-butyllithium; hydrogen; boron tribromide; palladium on activated charcoal; In tetrahydrofuran; pyridine; hexane; dichloromethane; tert-butyl alcohol; benzene;
DOI:10.1002/jps.2600720719

Reference yield:

: (2,3-dimethoxybenzyl)triphenylphosphonium bromide

: 76619-72-2
diacetyl-3-n-heptadecylcatechol

Guidance literature:: Multi-step reaction with 4 steps

1: n-BuLi / tetrahydrofuran; hexane / 16 h / Heating

2: H₂ / Pd-C / 2-methyl-propan-2-ol

3: 78 percent / BBr₃ / CH₂Cl₂

4: pyridine / 4 h / Ambient temperature

With n-butyllithium; hydrogen; boron tribromide; palladium on activated charcoal; In tetrahydrofuran; pyridine; hexane; dichloromethane; tert-butyl alcohol;
DOI:10.1002/jps.2600720719