BP4MPy , 3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl

Base Information

• Chemical Name: BP4MPy , 3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl
• CAS No.: 1009033-94-6
• Molecular Formula: C56H38N4
• Molecular Weight: 766.93
• Mol file: 1009033-94-6.mol

Synonyms:BP4MPy , 3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl;3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl

Chemical Property of BP4MPy , 3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl

Chemical Property:

• Melting Point: 191℃
• PSA: 51.56000
• LogP: 14.26960

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BP4MPy , 3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl

There total 1 articles about BP4MPy , 3,3',5,5'-tetra[(M-pyridyl)-phen-3-yl]biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)pyridine (939430-30-5) + 3,3',5,5'-tetrabromo-1,1'-biphenyl (16400-50-3) → 3,5,3',5'-tetra(m-pyridin-3-yl)phenyl-[1,1']biphenyl (1009033-94-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; for 24h; Inert atmosphere; Reflux;

DOI:10.1021/ol7030872

upstream raw materials:

3-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)pyridine

3,3',5,5'-tetrabromo-1,1'-biphenyl

Refernces