9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione

Base Information

Chemical Name:9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione
CAS No.:17756-29-5
Molecular Formula:C10H14N4OS
Molecular Weight:238.3094
Hs Code.:
DSSTox Substance ID:DTXSID00404706
NSC Number:90607

Synonyms:17756-29-5;NSC90607;NCIOpen2_005551;9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione;SCHEMBL8467559;DTXSID00404706;NSC-90607

Suppliers and Price of 9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione

Chemical Property:

Vapor Pressure:3.14E-11mmHg at 25°C
Boiling Point:510.1°Cat760mmHg
Flash Point:262.3°C
Density:1.42g/cm³
XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:238.08883226
Heavy Atom Count:16
Complexity:284

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=NC(=S)C2=C(N1)N(C=N2)CCCCCO

Technology Process of 9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione

There total 3 articles about 9-(5-Hydroxypentyl)-3,9-dihydro-6H-purine-6-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9-[5-(tert-Butyl-diphenyl-silanyloxy)-pentyl]-9H-purine-6-thiol

: 17756-29-5
6-Mercapto-9H-purin-9-yl-pentanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/jm960844m

Reference yield:

: 111-29-5
1 ,5-pentanediol

: 17756-29-5
6-Mercapto-9H-purin-9-yl-pentanol

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / CH₂Cl₂ / 2.25 h / 0 - 20 °C

2: 1.) PPh₃, DEAD / 1.) THF, 10 min, 2.) THF, RT, overnight

3: Bu₄NF / tetrahydrofuran

With tetrabutyl ammonium fluoride; sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm960844m

Reference yield:

: 121671-76-9
5-(tert-butyldiphenylsilyloxy)pentan-1-ol

: 17756-29-5
6-Mercapto-9H-purin-9-yl-pentanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) PPh₃, DEAD / 1.) THF, 10 min, 2.) THF, RT, overnight

2: Bu₄NF / tetrahydrofuran

With tetrabutyl ammonium fluoride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1021/jm960844m