tert-Butyl (2-(4-(((di-tert-butoxyphosphoryl)oxy)methoxy)-3-formylphenyl)-2-hydroxyethyl)(6-(4-phenylbutoxy)hexyl)carbamate

Base Information

• Chemical Name: tert-Butyl (2-(4-(((di-tert-butoxyphosphoryl)oxy)methoxy)-3-formylphenyl)-2-hydroxyethyl)(6-(4-phenylbutoxy)hexyl)carbamate
• CAS No.: 1034189-07-5
• Molecular Formula: C₃₉H₆₂NO₁₀P
• Molecular Weight: 735.896
• Mol file: 1034189-07-5.mol

Synonyms:

Chemical Property of tert-Butyl (2-(4-(((di-tert-butoxyphosphoryl)oxy)methoxy)-3-formylphenyl)-2-hydroxyethyl)(6-(4-phenylbutoxy)hexyl)carbamate

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-Butyl (2-(4-(((di-tert-butoxyphosphoryl)oxy)methoxy)-3-formylphenyl)-2-hydroxyethyl)(6-(4-phenylbutoxy)hexyl)carbamate

There total 2 articles about tert-Butyl (2-(4-(((di-tert-butoxyphosphoryl)oxy)methoxy)-3-formylphenyl)-2-hydroxyethyl)(6-(4-phenylbutoxy)hexyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[2-(3-formyl-4-hydroxy-phenyl)-2-hydroxy-ethyl]-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester (917480-06-9) + di-tert-butyl chloromethyl phosphate (229625-50-7) → {2-[4-(di-tert-butoxy-phosphoryloxymethoxy)-3-formyl-phenyl]-2-hydroxy-ethyl}-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester (1034189-07-5)

Guidance literature:

With sodium hydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 50 ℃; for 18h;

Reference yield:

[2-(3-formyl-4-hydroxy-phenyl)-2-hydroxy-ethyl]-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester (917480-06-9) + di-tert-butyl chloromethyl phosphate (229625-50-7) → {2-[4-(di-tert-butoxy-phosphoryloxymethoxy)-3-formyl-phenyl]-2-hydroxy-ethyl}-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester (1034189-07-5) + C35H54NO10P

Guidance literature:

With sodium hydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 50 ℃; for 18h;

Reference yield: 98.0%

{2-[4-(di-tert-butoxy-phosphoryloxymethoxy)-3-formyl-phenyl]-2-hydroxy-ethyl}-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester (1034189-07-5) → {2-[4-(di-tert-butoxy-phosphoryloxymethoxy)-3-hydroxymethyl-phenyl]-2-hydroxy-ethyl}-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester (1034189-09-7)

Guidance literature:

With methanol; sodium tetrahydroborate; In tetrahydrofuran; at -78 - 20 ℃; for 2h;

upstream raw materials:

[2-(3-formyl-4-hydroxy-phenyl)-2-hydroxy-ethyl]-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester

di-tert-butyl chloromethyl phosphate

Downstream raw materials:

{2-[4-(di-tert-butoxy-phosphoryloxymethoxy)-3-hydroxymethyl-phenyl]-2-hydroxy-ethyl}-[6-(4-phenyl-butoxy)-hexyl]-carbamic acid tert-butyl ester

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