tert-butyl (4-iodo-2-nitrophenyl)carbaMate

Base Information

• Chemical Name: tert-butyl (4-iodo-2-nitrophenyl)carbaMate
• CAS No.: 335254-69-8
• Molecular Formula: C11H13IN2O4
• Molecular Weight: 364.14
• Mol file: 335254-69-8.mol

Synonyms:N-Boc-4-iodo-2-nitroaniline;tert-butyl (4-iodo-2-nitrophenyl)carbaMate;(4-Iodo-2-nitrophenyl)carbamic acid tert-butyl ester

Chemical Property of tert-butyl (4-iodo-2-nitrophenyl)carbaMate

Chemical Property:

• PSA: 87.64000
• LogP: 4.08320
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl(4-iodo-2-nitrophenyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl (4-iodo-2-nitrophenyl)carbaMate

There total 6 articles about tert-butyl (4-iodo-2-nitrophenyl)carbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-[bis(tert-butoxycarbonyl)amino]-4-iodo-2-nitrobenzene → 1-(tert-butoxycarbonyl)amino-4-iodo-2-nitrobenzene (335254-69-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1039/c3md00110e

Reference yield: 50.0%

→ 1-(tert-butoxycarbonyl)amino-4-iodo-2-nitrobenzene (335254-69-8)

Guidance literature:

With dmap; lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 4-iodo-2-nitroaniline (20691-72-9) → 1-(tert-butoxycarbonyl)amino-4-iodo-2-nitrobenzene (335254-69-8)

Guidance literature:

With caesium carbonate; In methanol; hexane; water; butanone;

upstream raw materials:

di-tert-butyl dicarbonate

4-iodo-2-nitroaniline

2-nitro-aniline

tert-butyl alcohol

Downstream raw materials:

(2-nitro-4-pyridin-3-yl-phenyl)-carbamic acid tert.-butyl ester

tert-butyl 2-nitro-4-(pyridin-2-yl)phenylcarbamate

(2-nitro-4-pyridin-4-yl-phenyl)-carbamic acid tert.-butyl ester

tert-butyl (2-nitro-4-(thiophen-2-yl) phenyl)carbamate

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