1-Methyl-3-methoxycarbonyl-pyrrolidine

Base Information

• Chemical Name: 1-Methyl-3-methoxycarbonyl-pyrrolidine
• CAS No.: 34616-29-0
• Molecular Formula: C7H13NO2
• Molecular Weight: 143.1836
• Hs Code.: 2933990090
• Mol file: 34616-29-0.mol

Synonyms:3-Pyrrolidinecarboxylic acid, 1-methyl-, methyl ester;methyl 1-methylpyrrolidine-3-carboxylate

Chemical Property of 1-Methyl-3-methoxycarbonyl-pyrrolidine

Chemical Property:

• Vapor Pressure: 1.86mmHg at 25°C
• Boiling Point: 165.6°C at 760 mmHg
• PKA: 9.18±0.40(Predicted)
• Flash Point: 59.5°C
• PSA: 29.54000
• Density: 1.042g/cm³
• LogP: 0.04900
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl 1-methylpyrrolidine-3-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Methyl-3-methoxycarbonyl-pyrrolidine

There total 3 articles about 1-Methyl-3-methoxycarbonyl-pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + sarcosine (107-97-1,25951-24-0) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 1-Methyl-3-methoxycarbonyl-pyrrolidine (34616-29-0)

Guidance literature:

In benzene; for 3h; Heating;

Reference yield:

sarcosine (107-97-1,25951-24-0) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 1-Methyl-3-methoxycarbonyl-pyrrolidine (34616-29-0)

Guidance literature:

With paraformaldehyde; In toluene;

Reference yield:

→ 1-Methyl-3-methoxycarbonyl-pyrrolidine (34616-29-0)

Guidance literature:

10a, 1.) CrO3/H2SO4, Oxid., 2.) Me., HCl, Veresterung;

DOI:10.1021/jo00921a008

upstream raw materials:

formaldehyd

sarcosine

acrylic acid methyl ester

Downstream raw materials:

3-Methyl-5-(1-methyl-pyrrolidin-3-yl)-[1,2,4]oxadiazole

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