3,3-Dimethylazetidine hydrochloride

Base Information

• Chemical Name: 3,3-Dimethylazetidine hydrochloride
• CAS No.: 89381-03-3
• Molecular Formula: C5H12ClN
• Molecular Weight: 121.61
• Hs Code.: 2933990090
• Mol file: 89381-03-3.mol

Synonyms:3,3-DIMETHYLAZETIDINE HYDROCHLORIDE;3,3-DIMETHYLAZETIDINE HCL

Chemical Property of 3,3-Dimethylazetidine hydrochloride

Chemical Property:

• Melting Point: 96-98 °C
• PSA: 12.03000
• LogP: 1.74660
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3,3-dimethylazetidinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3-Dimethylazetidine hydrochloride

There total 2 articles about 3,3-Dimethylazetidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.7%

3,3-dimethyl-N-<4-methylphenylsulfonyl>azetidine (79201-18-6) → 3,3-dimethylazetidine hydrochloride (89381-03-3)

Guidance literature:

3,3-dimethyl-N-<4-methylphenylsulfonyl>azetidine; With pentan-1-ol; sodium; at 110 ℃;

With hydrogenchloride; In dichloromethane;

Reference yield: 24.7%

→ 3,3-dimethylazetidine hydrochloride (89381-03-3)

Guidance literature:

With hydrogenchloride; sodium chloride; In pentan-1-ol; water;

Reference yield: 70.0%

8-chloro-N-(2-ethoxy-4-(4-methyl-4H-1,2,4-triazol-3-yl)phenyl)-6-methylpyrido[3,4-d]pyrimidin-2-amine (1578246-82-8) + 3,3-dimethylazetidine hydrochloride (89381-03-3) → 8-(3,3-dimethylazetidin-1-yl)-N-(2-ethoxy-4-(4-methyl-4H-1,2,4-triazol-3-yl)phenyl)-6- methylpyrido[3,4-d]pyrimidin-2-amine

Guidance literature:

With triethylamine; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 18h; Sealed tube;

upstream raw materials:

3,3-dimethyl-N-<4-methylphenylsulfonyl>azetidine

Downstream raw materials:

1-(3,3-dimethylazetidin-1-yl)-2-[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]ethanone

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