3,3'-(2,6-Pyridinediyldicarbonyl)bis-2-thiazolidinethione

Base Information

• Chemical Name: 3,3'-(2,6-Pyridinediyldicarbonyl)bis-2-thiazolidinethione
• CAS No.: 156458-78-5
• Molecular Formula: C13H11N3O2S4
• Molecular Weight: 369.51
• Mol file: 156458-78-5.mol

Synonyms:3,3'-(2,6-PYRIDINEDIYLDICARBONYL)BIS-2-THIAZOLIDINETHIONE;

Chemical Property of 3,3'-(2,6-Pyridinediyldicarbonyl)bis-2-thiazolidinethione

Chemical Property:

• Boiling Point: 584.5±60.0 °C(Predicted)
• PKA: -1.40±0.10(Predicted)
• PSA: 168.29000
• Density: 1.66
• LogP: 1.90520

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: thiazolidin e thione pharmaceutical intermediate

Technology Process of 3,3'-(2,6-Pyridinediyldicarbonyl)bis-2-thiazolidinethione

There total 1 articles about 3,3'-(2,6-Pyridinediyldicarbonyl)bis-2-thiazolidinethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

thiazolidine-2-thione (134469-06-0) + 2,6-Pyridinedicarbonyl dichloride (3739-94-4) → N2,N6-di(2-thioxothiazolidin-3-yl)pyridine-2,6-dicarboxamide (156458-78-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 50 ℃; for 1h;

DOI:10.1016/S0040-4020(97)00896-X

Reference yield: 75.0%

1,2-diamino-benzene (95-54-5) + N2,N6-di(2-thioxothiazolidin-3-yl)pyridine-2,6-dicarboxamide (156458-78-5) → N2,N6'-bis(2-aminophenpy)pyridine-2,6-dicarboximide (373614-45-0)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1055/s-2001-16076

Reference yield: 30.0%

N5,N5'-bis(2-(aminomethyl)phenyl)-3,3'-dimethyl-4,4'-diphenyl-1H,1'H-[2,2'-bipyrrole]-5,5'-dicarboxamide (1429988-57-7) + N2,N6-di(2-thioxothiazolidin-3-yl)pyridine-2,6-dicarboxamide (156458-78-5) → 15,18,50,53-tetramethyl-14,19,49,54-tetraphenyl-3,11,22,30,38,46,57,65,71,72,73,74,75,76-tetradecaazaundecacyclo[65.3.1.1(13,16).1(17,20).1(32,36).1(48,51).1(52,55).0(5,10).0(23,28).0(40,45).0(58,63)]hexaheptaconta-1(71),5,7,9,13,15,17,19,23(28),24,26,32(74),33,35,40(45),41,43,48,50,52,54,58,60,62,67,69-hexacosaen-2,12,21,31,37,47,56,66-octone (1429988-58-8)

Guidance literature:

In chloroform;

DOI:10.1002/chem.201204306

upstream raw materials:

thiazolidine-2-thione

2,6-Pyridinedicarbonyl dichloride

Downstream raw materials:

N²,N⁶'-bis(2-aminophenpy)pyridine-2,6-dicarboximide

15,18,50,53-tetramethyl-14,19,49,54-tetraphenyl-3,11,22,30,38,46,57,65,71,72,73,74,75,76-tetradecaazaundecacyclo[65.3.1.1(13,16).1(17,20).1(32,36).1(48,51).1(52,55).0(5,10).0(23,28).0(40,45).0(58,63)]hexaheptaconta-1⁽⁷¹⁾,5,7,9,13,15,17,19,23⁽²⁸⁾,24,26,32⁽⁷⁴⁾,33,35,40⁽⁴⁵⁾,41,43,48,50,52,54,58,60,62,67,69-hexacosaen-2,12,21,31,37,47,56,66-octone

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