4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole

Base Information

Chemical Name:4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole
CAS No.:103483-02-9
Molecular Formula:C8H13NS2
Molecular Weight:187.33
Hs Code.:
Mol file:103483-02-9.mol

Synonyms:Thiazole, 4,5-dihydro-2-[(3-Methyl-2-butenyl)thio];4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole

Suppliers and Price of 4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole

Chemical Property:

Boiling Point:272℃
Flash Point:118℃
PSA：62.96000
Density:1.13
LogP:2.22420

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses thiazolidin e thione pharmaceutical intermediate

Technology Process of 4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole

There total 1 articles about 4,5-Dihydro-2-[(3-methyl-2-buten-1-yl)thio]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 134469-06-0
thiazolidine-2-thione

: 503-60-6
3,3-dimethyl-allyl chloride

: 103483-02-9
1-(4',5'-dihydrothiazol-2'-yl)thio-3-methylbut-2-ene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 10 ℃; 1.) 15 min, 2.) 15 min;
DOI:10.1007/BF00965388

Reference yield: 96.0%

: 116854-26-3
1,4-dibenzyloxy-2,3-dimethoxy-5-methyl-6-(36'-chloro-3',7',11',15',19',23',27',31',35'-nonamethylhexatriaconta-2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E-nonaenyl)benzene

: 103483-02-9
1-(4',5'-dihydrothiazol-2'-yl)thio-3-methylbut-2-ene

: 116854-27-4
1,4-dibenzyloxy-2,3-dimethoxy-5-methyl-6-<37'-(4'',5''-dihydrothiazol-2''-yl)thio-3',7',11',15',19',23',27',31',35',39'-decamethyltetraconta-2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'-decaenyl>benzene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 0.5h;
DOI:10.1007/BF00965388

Reference yield:

: 103483-02-9
1-(4',5'-dihydrothiazol-2'-yl)thio-3-methylbut-2-ene

: 303-98-0,55127-92-9
ubidecarenone

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1.) n-BuLi / tetrahydrofuran; hexane / 0.5 h / -70 °C

2: 1.) Li, NH₃, 2.) FeCl₃, air / 1.) Et₂O, -40 deg C, 3 h, 2.) AcOH, 25 deg C

With n-butyllithium; air; ammonia; iron(III) chloride; lithium; In tetrahydrofuran; hexane;
DOI:10.1007/BF00965388