1-Bromododecane-d25

Base Information

Chemical Name:1-Bromododecane-d25
CAS No.:204259-66-5
Molecular Formula:CD3(CD2)11Br
Molecular Weight:274.39
Hs Code.:
European Community (EC) Number:686-090-8
DSSTox Substance ID:DTXSID90583892
Nikkaji Number:J1.786.286C
Wikidata:Q72455214
Mol file:204259-66-5.mol

Synonyms:1-Bromododecane-d25;204259-66-5;1-bromo-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-pentacosadeuteriododecane;Lauryl bromide-d25;1-bromo(?H??)dodecane;1-Bromo(~2~H_25_)dodecane;DTXSID90583892;HY-W008758S;1-Bromododecane-d25, 98 atom % D;AKOS015913093;CS-0542596;D98280;J-013303

Suppliers and Price of 1-Bromododecane-d25

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
1-Bromododecane-d25 98 atom % D
1g
$ 654.00

Medical Isotopes, Inc.
1-Bromododecane-d25
1 g
$ 1540.00

Medical Isotopes, Inc.
1-Bromododecane-d25
0.5 g
$ 860.00

American Custom Chemicals Corporation
1-BROMODODECANE-D25 95.00%
5MG
$ 497.71

Total 7 raw suppliers

Chemical Property of 1-Bromododecane-d25

Chemical Property:

Vapor Pressure:0.00817mmHg at 25°C
Melting Point:-11--9oC(lit.)
Refractive Index:n20/D 1.458(lit.)
Boiling Point:134-135oC6 mm Hg(lit.)
Flash Point:113oC
PSA：0.00000
Density:1.141
LogP:5.30220
XLogP3:7.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:10
Exact Mass:273.27088
Heavy Atom Count:13
Complexity:81.2

Purity/Quality:

99% ^*data from raw suppliers

1-Bromododecane-d25 98 atom % D ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCBr
Isomeric SMILES:[2H]C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])C([2H])([2H])Br
Uses 1-Bromododecane-d25 (CAS# 204259-66-5) is a useful isotopically labeled research compound.

Technology Process of 1-Bromododecane-d25

There total 2 articles about 1-Bromododecane-d25 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 160776-83-0
d₂₅-n-dodecanol

: 204259-66-5,204259-68-7
Deuterated dodecyl bromide

Guidance literature:: With pyridine; phosphorus tribromide; at 150 - 160 ℃; for 3h;
DOI:10.1016/0584-8539(96)01680-7

Reference yield:

: 59154-43-7,1219804-38-2
lauric acid-d₂₃

: 204259-66-5,204259-68-7
Deuterated dodecyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlD₄ / tetrahydrofuran / 2.5 h / Heating

2: 85 percent / PBr₃, pyridine / 3 h / 150 - 160 °C

With pyridine; lithium aluminium deuteride; phosphorus tribromide; In tetrahydrofuran;
DOI:10.1016/0584-8539(96)01680-7

Reference yield:

: 204259-66-5,204259-68-7
Deuterated dodecyl bromide

: C₃₁H₃₁⁽²⁾H₂₅O₉S

Guidance literature:: Multi-step reaction with 2 steps

1: Na

2: Et₃N / CH₂Cl₂

With sodium; triethylamine; In dichloromethane;
DOI:10.1021/jp971330h