DI-N-HEXYL PHTHALATE-3,4,5,6-D4

Base Information

• Chemical Name: DI-N-HEXYL PHTHALATE-3,4,5,6-D4
• CAS No.: 1015854-55-3
• Molecular Formula: C6D4[COO(CH2)5CH3]2
• Molecular Weight: 338.48
• Mol file: 1015854-55-3.mol

Synonyms:Di-n-hexyl phthalate-d4;Dihexyl phthalate-3,4,5,6-d4;

Chemical Property of DI-N-HEXYL PHTHALATE-3,4,5,6-D4

Chemical Property:

• PSA: 52.60000
• LogP: 5.16080

Purity/Quality:

99% ^*data from raw suppliers

Dihexyl phthalate-3,4,5,6-d4 analytical standard ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 61
• Safety Statements: 53-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DI-N-HEXYL PHTHALATE-3,4,5,6-D4

There total 1 articles about DI-N-HEXYL PHTHALATE-3,4,5,6-D4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3,4,5,6-tetradeuterophtaloyl dicarboxylic acid (87976-26-9) + hexan-1-ol (111-27-3) → dihexyl phthalate-3,4,5,6-d4 (1015854-55-3)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/jlcr.3930

upstream raw materials:

3,4,5,6-tetradeuterophtaloyl dicarboxylic acid

hexan-1-ol

Refernces

• 1、 Xu, Zhongjie,Zhao, Cheng,Sun, Wen,Lei, Wen,Hu, Zuming. "An efficient and general method for the synthesis of stable isotope deuterium labeled phthalate esters". . p. 378 - 384. Retrieved 2021.